The synthesis of glucosinolates deuterium labelled in the glucose fragment

Avril A. B. Robertson, Nigel P. Botting

Research output: Contribution to journalArticlepeer-review

9 Citations (Scopus)

Abstract

A facile synthesis is described for 2,3,4,6-tetra-O-acetyl-thio-beta-D-[1-H-2,6-H-2(2)]glucopyranose, which has been used to make an isotopically labelled desulphoglucosinolate, [1'-H-2,6'-H-2(2)]desulfogluconasturtiln. This isotopically labelled building block can be employed to make any glucosinolate or desulfoglucosinolate for use as internal standards for MS based analytical methods. Copyright (c) 2006 John Wiley & Sons, Ltd.

Original languageEnglish
Pages (from-to)1201-1211
Number of pages11
JournalJournal of Labelled Compounds and Radiopharmaceuticals
Volume49
DOIs
Publication statusPublished - Nov 2006

Keywords

  • glucosinolates
  • isothiocyanates
  • gluconasturtiin
  • cancer prevention
  • CANCER PREVENTION
  • ISOTHIOCYANATES
  • VEGETABLES
  • APOPTOSIS
  • PRODUCTS

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