The preparation of a solubilised form of Lawessons Reagent and its thionation reactions.

MR Foreman; Alexandra Martha Zoya Slawin; John Derek Woollins

The preparation of a solubilised form of Lawessons Reagent and its thionation reactions.

MR Foreman, Alexandra Martha Zoya Slawin, John Derek Woollins

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Abstract

2-tert-Butylanisole and P4S10 react together to give 2,4-bis (3-tbutyl-4-methoxyphenyl) 1,3, 2, 4-dithiadiphosphetane 2, 4-disulfide (LR*) which was characterized by X-ray crystallography. Comparative thionation reactions of LR* and a range of P-S compounds were investigated. If was found that LR* in many cases, gives better yields of thionated complexes than Lawessons Reagent when the reactions are performed at room temperature. (C) 1999 John Wiley & Sons, Inc.

Original language	English
Volume	10
Publication status	Published - 1999

Keywords

HETEROCYCLES

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title = "The preparation of a solubilised form of Lawessons Reagent and its thionation reactions.",

abstract = "2-tert-Butylanisole and P4S10 react together to give 2,4-bis (3-tbutyl-4-methoxyphenyl) 1,3, 2, 4-dithiadiphosphetane 2, 4-disulfide (LR*) which was characterized by X-ray crystallography. Comparative thionation reactions of LR* and a range of P-S compounds were investigated. If was found that LR* in many cases, gives better yields of thionated complexes than Lawessons Reagent when the reactions are performed at room temperature. (C) 1999 John Wiley \& Sons, Inc.",

keywords = "HETEROCYCLES",

author = "MR Foreman and Slawin, \{Alexandra Martha Zoya\} and Woollins, \{John Derek\}",

note = "Heteroatom Chem",

year = "1999",

language = "English",

volume = "10",

type = "Other",

}

TY - GEN

T1 - The preparation of a solubilised form of Lawessons Reagent and its thionation reactions.

AU - Foreman, MR

AU - Slawin, Alexandra Martha Zoya

AU - Woollins, John Derek

N1 - Heteroatom Chem

PY - 1999

Y1 - 1999

N2 - 2-tert-Butylanisole and P4S10 react together to give 2,4-bis (3-tbutyl-4-methoxyphenyl) 1,3, 2, 4-dithiadiphosphetane 2, 4-disulfide (LR*) which was characterized by X-ray crystallography. Comparative thionation reactions of LR* and a range of P-S compounds were investigated. If was found that LR* in many cases, gives better yields of thionated complexes than Lawessons Reagent when the reactions are performed at room temperature. (C) 1999 John Wiley & Sons, Inc.

AB - 2-tert-Butylanisole and P4S10 react together to give 2,4-bis (3-tbutyl-4-methoxyphenyl) 1,3, 2, 4-dithiadiphosphetane 2, 4-disulfide (LR*) which was characterized by X-ray crystallography. Comparative thionation reactions of LR* and a range of P-S compounds were investigated. If was found that LR* in many cases, gives better yields of thionated complexes than Lawessons Reagent when the reactions are performed at room temperature. (C) 1999 John Wiley & Sons, Inc.

KW - HETEROCYCLES

UR - https://www.scopus.com/pages/publications/0141573057

M3 - Other contribution

VL - 10

ER -

The preparation of a solubilised form of Lawessons Reagent and its thionation reactions.

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