The preparation of a solubilised form of Lawessons Reagent and its thionation reactions.

MR Foreman, Alexandra Martha Zoya Slawin, John Derek Woollins

Research output: Other contribution

13 Citations (Scopus)

Abstract

2-tert-Butylanisole and P4S10 react together to give 2,4-bis (3-tbutyl-4-methoxyphenyl) 1,3, 2, 4-dithiadiphosphetane 2, 4-disulfide (LR*) which was characterized by X-ray crystallography. Comparative thionation reactions of LR* and a range of P-S compounds were investigated. If was found that LR* in many cases, gives better yields of thionated complexes than Lawessons Reagent when the reactions are performed at room temperature. (C) 1999 John Wiley & Sons, Inc.

Original languageEnglish
Volume10
Publication statusPublished - 1999

Keywords

  • HETEROCYCLES

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