TY - JOUR
T1 - The preparation and structures of Ph2P(E)OH and Ph2P(E)OP(E)Ph-2 (E=S, Se)
AU - Pilkington, M J
AU - Slawin, A M Z
AU - Williams, D J
AU - Woollins, J D
PY - 1995
Y1 - 1995
N2 - The preparation and characterization of the title compounds is reported. The selenium compounds have been characterized by x-ray crystallography. Ph2P(Se)OH 1 Pbca a = 6.203(1), b = 16.949(4), c = 22.939(5) Angstrom, Z = 8, 1523 observed data, R = 0.033, R-w = 0.038. Ph2P(Se)OP(Se)Ph(2)2 C2/c a = 15.426(4), b = 9.232(3), c = 18.027(5) Angstrom, beta = 118.40(2)degrees, Z = 4, 1446 observed data, R = 0.028, R-w = 0.030.
AB - The preparation and characterization of the title compounds is reported. The selenium compounds have been characterized by x-ray crystallography. Ph2P(Se)OH 1 Pbca a = 6.203(1), b = 16.949(4), c = 22.939(5) Angstrom, Z = 8, 1523 observed data, R = 0.033, R-w = 0.038. Ph2P(Se)OP(Se)Ph(2)2 C2/c a = 15.426(4), b = 9.232(3), c = 18.027(5) Angstrom, beta = 118.40(2)degrees, Z = 4, 1446 observed data, R = 0.028, R-w = 0.030.
KW - PLATINUM
U2 - 10.1080/13583149512331338345
DO - 10.1080/13583149512331338345
M3 - Article
SN - 1024-1221
VL - 1
SP - 145
EP - 151
JO - Main Group Chemistry
JF - Main Group Chemistry
IS - 1
ER -