Synthesis of new cyclic thionosulfites

E Zysman-Colman; CB Abrams; DN Harpp

doi:10.1021/jo0346306

Synthesis of new cyclic thionosulfites

E Zysman-Colman, CB Abrams, DN Harpp^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

19 Citations (Scopus)

Abstract

The reaction of a series of 1,2-diols with S2Cl2, 1,1'-thiobisbenzimidazole (4a), and 1,1'-dithiobisbenzimidazole (4b) provides the corresponding thionosulfites, ROS(S)OR (2), in moderate to good yield.

Original language	English
Pages (from-to)	7059-7062
Number of pages	4
Journal	The Journal of Organic Chemistry
Volume	68
Issue number	18
DOIs	https://doi.org/10.1021/jo0346306
Publication status	Published - 5 Sept 2003

Keywords

SULFUR MONOFLUORIDE
DIALKOXY DISULFIDES
MOLECULAR-STRUCTURE
MICROWAVE SPECTRUM
DYNAMIC NMR
ROTATION
CRYSTAL
REAGENTS
ISOMERS
ESTERS

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title = "Synthesis of new cyclic thionosulfites",

abstract = "The reaction of a series of 1,2-diols with S2Cl2, 1,1'-thiobisbenzimidazole (4a), and 1,1'-dithiobisbenzimidazole (4b) provides the corresponding thionosulfites, ROS(S)OR (2), in moderate to good yield.",

keywords = "SULFUR MONOFLUORIDE, DIALKOXY DISULFIDES, MOLECULAR-STRUCTURE, MICROWAVE SPECTRUM, DYNAMIC NMR, ROTATION, CRYSTAL, REAGENTS, ISOMERS, ESTERS",

author = "E Zysman-Colman and CB Abrams and DN Harpp",

year = "2003",

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doi = "10.1021/jo0346306",

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volume = "68",

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journal = "The Journal of Organic Chemistry",

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TY - JOUR

T1 - Synthesis of new cyclic thionosulfites

AU - Zysman-Colman, E

AU - Abrams, CB

AU - Harpp, DN

PY - 2003/9/5

Y1 - 2003/9/5

N2 - The reaction of a series of 1,2-diols with S2Cl2, 1,1'-thiobisbenzimidazole (4a), and 1,1'-dithiobisbenzimidazole (4b) provides the corresponding thionosulfites, ROS(S)OR (2), in moderate to good yield.

AB - The reaction of a series of 1,2-diols with S2Cl2, 1,1'-thiobisbenzimidazole (4a), and 1,1'-dithiobisbenzimidazole (4b) provides the corresponding thionosulfites, ROS(S)OR (2), in moderate to good yield.

KW - SULFUR MONOFLUORIDE

KW - DIALKOXY DISULFIDES

KW - MOLECULAR-STRUCTURE

KW - MICROWAVE SPECTRUM

KW - DYNAMIC NMR

KW - ROTATION

KW - CRYSTAL

KW - REAGENTS

KW - ISOMERS

KW - ESTERS

U2 - 10.1021/jo0346306

DO - 10.1021/jo0346306

M3 - Article

SN - 0022-3263

VL - 68

SP - 7059

EP - 7062

JO - The Journal of Organic Chemistry

JF - The Journal of Organic Chemistry

IS - 18

ER -

Synthesis of new cyclic thionosulfites

Abstract

Keywords

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