Synthesis Of Deuterium Labelled Desulfoglucosinolates as Internal Standards for LC-MS Analysis

Nigel Peter Botting, AAB Robertson

Research output: Contribution to journalArticlepeer-review

19 Citations (Scopus)

Abstract

The syntheses of three deuterium labelled desulfoglucosinolates are described. These are the phenethyl, 1-methoxyindolyl and 4-methoxyindolyl derivatives. The compounds were prepared as internal standards for use in the quantitative LC-MS analysis of glucosinolates to improve the sensitivity of the analytical procedure. (C) 1999 Elsevier Science Ltd. All rights reserved.

Original languageEnglish
Pages (from-to)13269-13284
Number of pages16
JournalTetrahedron
Volume55
Publication statusPublished - 12 Nov 1999

Keywords

  • thioglycosides
  • labelling
  • plants
  • insects
  • FLY DELIA-FLORALIS
  • OVIPOSITION
  • PLANTS

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