Synthesis and structure of all-syn-1,2,3,4-tetrafluorocyclohexane

Alastair J. Durie, Alexandra M. Z. Slawin, Tomas Lebl, Peer Kirschb, David O'Hagan

Research output: Contribution to journalArticlepeer-review

39 Citations (Scopus)

Abstract

Preparation of the all-syn isomer of 1,2,3,4-tetrafluorocyclohexane is reported; X-ray structural studies shows a conformation with two of the C-F bonds oriented 1,3-diaxial to each other and F-19-NMR reveals a through space diaxial (4)J(FF) coupling constant of 29 Hz.

Original languageEnglish
Pages (from-to)8265-8267
Number of pages3
JournalChemical Communications
Volume47
Issue number29
Early online date28 Jun 2011
DOIs
Publication statusPublished - 7 Aug 2011

Keywords

  • FLUORINE
  • CHEMISTRY
  • COMPLEX
  • BOND

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