STRUCTURE OF 1-BUTYL-5-[(4-CHLOROPHENYL)AZO]-1,2,5,6-TETRAHYDRO-4-METHYL-2,6-DIOXO-3-PYRIDINECARBONITRILE

S N  BLACK; R J  DAVEY; A M Z  SLAWIN; D J  WILLIAMS

STRUCTURE OF 1-BUTYL-5-[(4-CHLOROPHENYL)AZO]-1,2,5,6-TETRAHYDRO-4-METHYL-2,6-DIOXO-3-PYRIDINECARBONITRILE

S N BLACK, R J DAVEY, A M Z SLAWIN, D J WILLIAMS

Research output: Contribution to journal › Article › peer-review

Abstract

C17H17ClN4O2, M(r) = 344.8, monoclinic, P2(1)/c, a = 7.586 (2), b = 11.429 (4), c = 19.592 (8) angstrom, beta = 93.52 (3)-degrees, V = 1695 (1) angstrom 3, Z = 4, D(x) = 1.35 Mg m-3, Cu K-alpha radiation, lambda = 1.54178 angstrom, mu = 2.19 mm-1, F(000) = 776, room temperature, R = 0.045 for 1499 observed reflections with \F(omicron)\ > 3-sigma(\F(omicron)\). The molecule has an essentially planar and highly conjugated geometry reinforced by an intra-molecular NH...O hydrogen bond. The molecules form parallel overlapping stacks in the crystal.

Original language	English
Pages (from-to)	323-325
Number of pages	3
Journal	Acta Crystallographica Section C: Crystal Structure Communications
Volume	48
Publication status	Published - 15 Feb 1992

Cite this

@article{63e6ae4681da40f187a5c838a6949c1e,

title = "STRUCTURE OF 1-BUTYL-5-[(4-CHLOROPHENYL)AZO]-1,2,5,6-TETRAHYDRO-4-METHYL-2,6-DIOXO-3-PYRIDINECARBONITRILE",

abstract = "C17H17ClN4O2, M(r) = 344.8, monoclinic, P2(1)/c, a = 7.586 (2), b = 11.429 (4), c = 19.592 (8) angstrom, beta = 93.52 (3)-degrees, V = 1695 (1) angstrom 3, Z = 4, D(x) = 1.35 Mg m-3, Cu K-alpha radiation, lambda = 1.54178 angstrom, mu = 2.19 mm-1, F(000) = 776, room temperature, R = 0.045 for 1499 observed reflections with \textbackslash{}F(omicron)\textbackslash{} > 3-sigma(\textbackslash{}F(omicron)\textbackslash{}). The molecule has an essentially planar and highly conjugated geometry reinforced by an intra-molecular NH...O hydrogen bond. The molecules form parallel overlapping stacks in the crystal.",

author = "BLACK, \{S N\} and DAVEY, \{R J\} and SLAWIN, \{A M Z\} and WILLIAMS, \{D J\}",

year = "1992",

month = feb,

day = "15",

language = "English",

volume = "48",

pages = "323--325",

journal = "Acta Crystallographica Section C: Crystal Structure Communications",

issn = "0108-2701",

publisher = "International Union of Crystallography",

}

TY - JOUR

T1 - STRUCTURE OF 1-BUTYL-5-[(4-CHLOROPHENYL)AZO]-1,2,5,6-TETRAHYDRO-4-METHYL-2,6-DIOXO-3-PYRIDINECARBONITRILE

AU - BLACK, S N

AU - DAVEY, R J

AU - SLAWIN, A M Z

AU - WILLIAMS, D J

PY - 1992/2/15

Y1 - 1992/2/15

N2 - C17H17ClN4O2, M(r) = 344.8, monoclinic, P2(1)/c, a = 7.586 (2), b = 11.429 (4), c = 19.592 (8) angstrom, beta = 93.52 (3)-degrees, V = 1695 (1) angstrom 3, Z = 4, D(x) = 1.35 Mg m-3, Cu K-alpha radiation, lambda = 1.54178 angstrom, mu = 2.19 mm-1, F(000) = 776, room temperature, R = 0.045 for 1499 observed reflections with \F(omicron)\ > 3-sigma(\F(omicron)\). The molecule has an essentially planar and highly conjugated geometry reinforced by an intra-molecular NH...O hydrogen bond. The molecules form parallel overlapping stacks in the crystal.

AB - C17H17ClN4O2, M(r) = 344.8, monoclinic, P2(1)/c, a = 7.586 (2), b = 11.429 (4), c = 19.592 (8) angstrom, beta = 93.52 (3)-degrees, V = 1695 (1) angstrom 3, Z = 4, D(x) = 1.35 Mg m-3, Cu K-alpha radiation, lambda = 1.54178 angstrom, mu = 2.19 mm-1, F(000) = 776, room temperature, R = 0.045 for 1499 observed reflections with \F(omicron)\ > 3-sigma(\F(omicron)\). The molecule has an essentially planar and highly conjugated geometry reinforced by an intra-molecular NH...O hydrogen bond. The molecules form parallel overlapping stacks in the crystal.

UR - https://www.scopus.com/pages/publications/37049088711

M3 - Article

SN - 0108-2701

VL - 48

SP - 323

EP - 325

JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

ER -

STRUCTURE OF 1-BUTYL-5-[(4-CHLOROPHENYL)AZO]-1,2,5,6-TETRAHYDRO-4-METHYL-2,6-DIOXO-3-PYRIDINECARBONITRILE

Abstract

Other files and links

Fingerprint

Cite this