Racemic cis-methoxobis(2-methyl-3-oxo-4H-pyran-4-olato)oxovanadium(V) redetermined at 120 K: hydrogen-bonded ribbons containing R-2(2)(7), R-2(2)(14) and R-4(4)(18) rings

S J Kavitha, K A B Panchanatheswaran, J N Low, C Glidewell

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Abstract

In the title compound, [V(CH3O)(C6H5O3)(2)O], the V - O bond lengths to the oxo and methoxo ligands are 1.593 ( 3) and 1.768 (3) angstrom, respectively, at 120 K; the V - O bond lengths trans to these two ligands are 2.246 ( 3) and 2.116 ( 3) angstrom. Molecules are linked by three C - H center dot center dot center dot O hydrogen bonds into complex ribbons containing three types of ring.

Original languageEnglish
Number of pages3
JournalActa Crystallographica Section C-Crystal Structure Communications
Volume62
DOIs
Publication statusPublished - Mar 2006

Keywords

  • X-RAY
  • BIS(MALTOLATO)OXOVANADIUM(IV)
  • DIFFRACTION
  • COMPLEXES

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