Preparation and X-ray structure of a new organo-P–O–S heterocycle

M R S  FOREMAN; A M  SLAWIN; J D  WOOLLINS

doi:10.1039/C39950002217

Preparation and X-ray structure of a new organo-P–O–S heterocycle

M R S FOREMAN, A M SLAWIN, J D WOOLLINS

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Abstract

Reaction of 1,3-epithio-1 lambda(5),3 lambda(5)-naphtho[1,8-cd][1,2,6]thiadiphohosphinine-1,3-dithione 5 with 3,5-di-tert-butylcatechol gives 3,5-di-tert-butyl-1,8-epithio-1 lambda(5),8 lambda(5)-naphtho[1,8 -cd][1,7,2,6]benzodioxadiphosphonine-1,8-dithione 7 which, from X-ray studies, contains fused C3P2S and C2O2P2S rings.

Original language	English
Pages (from-to)	2217-2218
Number of pages	2
Journal	Journal of the Chemical Society, Chemical Communications
Issue number	21
DOIs	https://doi.org/10.1039/C39950002217
Publication status	Published - 7 Nov 1995

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title = "Preparation and X-ray structure of a new organo-P–O–S heterocycle",

abstract = "Reaction of 1,3-epithio-1 lambda(5),3 lambda(5)-naphtho[1,8-cd][1,2,6]thiadiphohosphinine-1,3-dithione 5 with 3,5-di-tert-butylcatechol gives 3,5-di-tert-butyl-1,8-epithio-1 lambda(5),8 lambda(5)-naphtho[1,8 -cd][1,7,2,6]benzodioxadiphosphonine-1,8-dithione 7 which, from X-ray studies, contains fused C3P2S and C2O2P2S rings.",

author = "FOREMAN, {M R S} and SLAWIN, {A M} and WOOLLINS, {J D}",

year = "1995",

month = nov,

day = "7",

doi = "10.1039/C39950002217",

language = "English",

pages = "2217--2218",

journal = "Journal of the Chemical Society, Chemical Communications",

issn = "0022-4936",

publisher = "Chemical Society",

number = "21",

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TY - JOUR

T1 - Preparation and X-ray structure of a new organo-P–O–S heterocycle

AU - FOREMAN, M R S

AU - SLAWIN, A M

AU - WOOLLINS, J D

PY - 1995/11/7

Y1 - 1995/11/7

N2 - Reaction of 1,3-epithio-1 lambda(5),3 lambda(5)-naphtho[1,8-cd][1,2,6]thiadiphohosphinine-1,3-dithione 5 with 3,5-di-tert-butylcatechol gives 3,5-di-tert-butyl-1,8-epithio-1 lambda(5),8 lambda(5)-naphtho[1,8 -cd][1,7,2,6]benzodioxadiphosphonine-1,8-dithione 7 which, from X-ray studies, contains fused C3P2S and C2O2P2S rings.

AB - Reaction of 1,3-epithio-1 lambda(5),3 lambda(5)-naphtho[1,8-cd][1,2,6]thiadiphohosphinine-1,3-dithione 5 with 3,5-di-tert-butylcatechol gives 3,5-di-tert-butyl-1,8-epithio-1 lambda(5),8 lambda(5)-naphtho[1,8 -cd][1,7,2,6]benzodioxadiphosphonine-1,8-dithione 7 which, from X-ray studies, contains fused C3P2S and C2O2P2S rings.

U2 - 10.1039/C39950002217

DO - 10.1039/C39950002217

M3 - Article

SN - 0022-4936

SP - 2217

EP - 2218

JO - Journal of the Chemical Society, Chemical Communications

JF - Journal of the Chemical Society, Chemical Communications

IS - 21

ER -

Preparation and X-ray structure of a new organo-P–O–S heterocycle

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