PREPARATION AND X-RAY STRUCTURE OF 1,4,2,3,5,6-DITHIATETRAZINE

J  NOVOSAD; D J  WILLIAMS; J D  WOOLLINS

PREPARATION AND X-RAY STRUCTURE OF 1,4,2,3,5,6-DITHIATETRAZINE

J NOVOSAD, D J WILLIAMS, J D WOOLLINS

Research output: Contribution to journal › Article › peer-review

Abstract

Reaction of sulfur dichloride with sym-EtO2CNHNHCO2Et 1 gives the title ring system which has been characterised by microanalyses, nmr, and X-Ray crystallography. The X-ray structure Of S2[N(CO2Et)]4 2 reveals that the S2N4 ring adopts a chair conformation with all four ester groups in pseudo-axial positions. Bond lengths and angles are compared with 1 and S4(NR)2.

Original language	English
Pages (from-to)	495-497
Number of pages	3
Journal	Zeitschrift für Anorganische und Allgemeine Chemie
Volume	620
Issue number	3
Publication status	Published - Mar 1994

Keywords

DITHIATETRAZINE
SYNTHESIS
CRYSTAL STRUCTURE
CRYSTAL

Cite this

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title = "PREPARATION AND X-RAY STRUCTURE OF 1,4,2,3,5,6-DITHIATETRAZINE",

abstract = "Reaction of sulfur dichloride with sym-EtO2CNHNHCO2Et 1 gives the title ring system which has been characterised by microanalyses, nmr, and X-Ray crystallography. The X-ray structure Of S2[N(CO2Et)]4 2 reveals that the S2N4 ring adopts a chair conformation with all four ester groups in pseudo-axial positions. Bond lengths and angles are compared with 1 and S4(NR)2.",

keywords = "DITHIATETRAZINE, SYNTHESIS, CRYSTAL STRUCTURE, CRYSTAL",

author = "J NOVOSAD and WILLIAMS, {D J} and WOOLLINS, {J D}",

year = "1994",

month = mar,

language = "English",

volume = "620",

pages = "495--497",

journal = "Zeitschrift f{\"u}r Anorganische und Allgemeine Chemie",

issn = "0044-2313",

publisher = "Wiley-VCH, Weinheim",

number = "3",

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TY - JOUR

T1 - PREPARATION AND X-RAY STRUCTURE OF 1,4,2,3,5,6-DITHIATETRAZINE

AU - NOVOSAD, J

AU - WILLIAMS, D J

AU - WOOLLINS, J D

PY - 1994/3

Y1 - 1994/3

N2 - Reaction of sulfur dichloride with sym-EtO2CNHNHCO2Et 1 gives the title ring system which has been characterised by microanalyses, nmr, and X-Ray crystallography. The X-ray structure Of S2[N(CO2Et)]4 2 reveals that the S2N4 ring adopts a chair conformation with all four ester groups in pseudo-axial positions. Bond lengths and angles are compared with 1 and S4(NR)2.

AB - Reaction of sulfur dichloride with sym-EtO2CNHNHCO2Et 1 gives the title ring system which has been characterised by microanalyses, nmr, and X-Ray crystallography. The X-ray structure Of S2[N(CO2Et)]4 2 reveals that the S2N4 ring adopts a chair conformation with all four ester groups in pseudo-axial positions. Bond lengths and angles are compared with 1 and S4(NR)2.

KW - DITHIATETRAZINE

KW - SYNTHESIS

KW - CRYSTAL STRUCTURE

KW - CRYSTAL

M3 - Article

SN - 0044-2313

VL - 620

SP - 495

EP - 497

JO - Zeitschrift für Anorganische und Allgemeine Chemie

JF - Zeitschrift für Anorganische und Allgemeine Chemie

IS - 3

ER -

PREPARATION AND X-RAY STRUCTURE OF 1,4,2,3,5,6-DITHIATETRAZINE

Abstract

Keywords

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