PREPARATION AND X-RAY STRUCTURE OF 1,4,2,3,5,6-DITHIATETRAZINE

J NOVOSAD, D J WILLIAMS, J D WOOLLINS

Research output: Contribution to journalArticlepeer-review

2 Citations (Scopus)

Abstract

Reaction of sulfur dichloride with sym-EtO2CNHNHCO2Et 1 gives the title ring system which has been characterised by microanalyses, nmr, and X-Ray crystallography. The X-ray structure Of S2[N(CO2Et)]4 2 reveals that the S2N4 ring adopts a chair conformation with all four ester groups in pseudo-axial positions. Bond lengths and angles are compared with 1 and S4(NR)2.

Original languageEnglish
Pages (from-to)495-497
Number of pages3
JournalZeitschrift für Anorganische und Allgemeine Chemie
Volume620
Issue number3
Publication statusPublished - Mar 1994

Keywords

  • DITHIATETRAZINE
  • SYNTHESIS
  • CRYSTAL STRUCTURE
  • CRYSTAL

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