Porous crystalline iron oxide thin films templated by mesoporous silica

K Y Shi; L M Peng; Q Chen; R H Wang; Wuzong Zhou

doi:10.1016/j.micromeso.2005.01.020

Porous crystalline iron oxide thin films templated by mesoporous silica

K Y Shi, L M Peng, Q Chen, R H Wang, Wuzong Zhou

Research output: Contribution to journal › Article › peer-review

Abstract

Continuous thin films of SBA-16 mesoporous silica with three-dimensional accessible pore structures (space group Im (3) over barm) have been prepared on indium-tin oxide glass (ITO) via a dip-coating technique using F-127 surfactants as the structure-directing agent in the non-aqueous media and under acidic conditions. The porous film was then used as a template to produce three-dimensional porous crystals of iron oxide by electrochemical deposition of iron metal followed by in-situ oxidation. Scanning electron microscopic images revealed several morphologies of the porous gamma-Fe2O3 particles. The detailed structures of these particles were examined by electron diffraction and high resolution transmission electron microscopy. (c) 2005 Published by Elsevier Inc.

Original language	English
Pages (from-to)	219-224
Number of pages	6
Journal	Microporous and Mesoporous Materials
Volume	83
DOIs	https://doi.org/10.1016/j.micromeso.2005.01.020
Publication status	Published - 1 Sept 2005

Keywords

mesoporous iron oxide
electron microscopy
thin film
SBA-16
nanostructure
COPOLYMER

Access to Document

10.1016/j.micromeso.2005.01.020

Cite this

@article{12b3b17d1b0248f5b84076307e31ea8d,

title = "Porous crystalline iron oxide thin films templated by mesoporous silica",

abstract = "Continuous thin films of SBA-16 mesoporous silica with three-dimensional accessible pore structures (space group Im (3) over barm) have been prepared on indium-tin oxide glass (ITO) via a dip-coating technique using F-127 surfactants as the structure-directing agent in the non-aqueous media and under acidic conditions. The porous film was then used as a template to produce three-dimensional porous crystals of iron oxide by electrochemical deposition of iron metal followed by in-situ oxidation. Scanning electron microscopic images revealed several morphologies of the porous gamma-Fe2O3 particles. The detailed structures of these particles were examined by electron diffraction and high resolution transmission electron microscopy. (c) 2005 Published by Elsevier Inc.",

keywords = "mesoporous iron oxide, electron microscopy, thin film, SBA-16, nanostructure, COPOLYMER",

author = "Shi, {K Y} and Peng, {L M} and Q Chen and Wang, {R H} and Wuzong Zhou",

year = "2005",

month = sep,

day = "1",

doi = "10.1016/j.micromeso.2005.01.020",

language = "English",

volume = "83",

pages = "219--224",

journal = "Microporous and Mesoporous Materials",

issn = "1387-1811",

publisher = "Elsevier",

}

TY - JOUR

T1 - Porous crystalline iron oxide thin films templated by mesoporous silica

AU - Shi, K Y

AU - Peng, L M

AU - Chen, Q

AU - Wang, R H

AU - Zhou, Wuzong

PY - 2005/9/1

Y1 - 2005/9/1

N2 - Continuous thin films of SBA-16 mesoporous silica with three-dimensional accessible pore structures (space group Im (3) over barm) have been prepared on indium-tin oxide glass (ITO) via a dip-coating technique using F-127 surfactants as the structure-directing agent in the non-aqueous media and under acidic conditions. The porous film was then used as a template to produce three-dimensional porous crystals of iron oxide by electrochemical deposition of iron metal followed by in-situ oxidation. Scanning electron microscopic images revealed several morphologies of the porous gamma-Fe2O3 particles. The detailed structures of these particles were examined by electron diffraction and high resolution transmission electron microscopy. (c) 2005 Published by Elsevier Inc.

AB - Continuous thin films of SBA-16 mesoporous silica with three-dimensional accessible pore structures (space group Im (3) over barm) have been prepared on indium-tin oxide glass (ITO) via a dip-coating technique using F-127 surfactants as the structure-directing agent in the non-aqueous media and under acidic conditions. The porous film was then used as a template to produce three-dimensional porous crystals of iron oxide by electrochemical deposition of iron metal followed by in-situ oxidation. Scanning electron microscopic images revealed several morphologies of the porous gamma-Fe2O3 particles. The detailed structures of these particles were examined by electron diffraction and high resolution transmission electron microscopy. (c) 2005 Published by Elsevier Inc.

KW - mesoporous iron oxide

KW - electron microscopy

KW - thin film

KW - SBA-16

KW - nanostructure

KW - COPOLYMER

UR - http://www.scopus.com/inward/record.url?scp=28844457601&partnerID=8YFLogxK

U2 - 10.1016/j.micromeso.2005.01.020

DO - 10.1016/j.micromeso.2005.01.020

M3 - Article

SN - 1387-1811

VL - 83

SP - 219

EP - 224

JO - Microporous and Mesoporous Materials

JF - Microporous and Mesoporous Materials

ER -

Porous crystalline iron oxide thin films templated by mesoporous silica

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

3D POROUS CRYSTALS OF TRANS METAL OX: 3D POROUS CRYSTALS OF TRANSITION

Cite this

Porous crystalline iron oxide thin films templated by mesoporous silica

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Projects

3D POROUS CRYSTALS OF TRANS METAL OX: 3D POROUS CRYSTALS OF TRANSITION

Cite this