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We report the development of a radical-polar cross-coupling reaction using styrene boronic acids and redox-active esters under organophotoredox catalysis. The reaction proceeds through a formal polarity-mismatched radical addition. The use of an organic photocatalyst enabled very low loadings of the electron-shuttle additive and accelerated reaction times compared to established processes. The scope of the reaction is explored, and the utility of the products is demonstrated.
- Styrylboronic acids
- Radical-polar cross-coupling
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Dataset underpinning "Organophotocatalytic Radical-Polar Cross-Coupling of Styrene Boronic Acids and Redox-Active Esters"
Watson, A. J. B. (Creator), University of St Andrews, 9 Nov 2023