Novel direct synthesis of mesoporous tin dioxide network intact up to 500°C

Tariq Aqeel; Heather F. Greer; Wuzong Zhou; Duncan W. Bruce; Ali Bumajdad

doi:10.4028/www.scientific.net/JNanoR.40.79

Novel direct synthesis of mesoporous tin dioxide network intact up to 500°C

Tariq Aqeel
, Heather F. Greer
, Wuzong Zhou
, Duncan W. Bruce
, Ali Bumajdad

Research output: Contribution to journal › Article › peer-review

Abstract

We present a direct soft templating method to synthesise mesoporous tin dioxide network that maintains a porous structure after calcination at 400 °C and 500 °C and has a relatively high BET surface area of 220 and 100 m² g^-1, respectively. TEM, BET and XRD results confirm that both crystal and pore sizes increase as a result of increasing the temperatures during the calcination step. This method is highly reproducible.

Original language	English
Pages (from-to)	79-89
Number of pages	11
Journal	Journal of Nano Research
Volume	40
Early online date	Mar 2016
DOIs	https://doi.org/10.4028/www.scientific.net/JNanoR.40.79
Publication status	E-pub ahead of print - Mar 2016

Keywords

Mesoporous tin dioxide
TEM
BET
XRD
XPS
Pore and crystal sizes
Calcinations

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10.4028/www.scientific.net/JNanoR.40.79

Zhou_MesoporousTinDioxide_JoNR_AM
Copyright © 2016, Trans Tech Publications Ltd.. This work is made available online in accordance with the publisher’s policies. This is the author created, accepted version manuscript following peer review and may differ slightly from the final published version. The final published version of this work is available at https://dx.doi.org/10.4028/www.scientific.net/JNanoR.40.79
Accepted author manuscript, 2.96 MB

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Energy Materials Discovery: Energy Materials Discovery Characterisation and Application
Irvine, J. (PI), Cassidy, M. (CoI), Connor, P. (CoI), Savaniu, C. (CoI) & Zhou, W. (CoI)
EPSRC
7/01/13 → 6/01/18
Project: Standard
EP/F019580/1 - Electron Microscopy: Electron Microscopy of Advanced Materials
Zhou, W. (PI), Irvine, J. (CoI) & Miller, A. (CoI)
EPSRC
1/10/07 → 31/03/12
Project: Standard

Cite this

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title = "Novel direct synthesis of mesoporous tin dioxide network intact up to 500°C",

abstract = "We present a direct soft templating method to synthesise mesoporous tin dioxide network that maintains a porous structure after calcination at 400 °C and 500 °C and has a relatively high BET surface area of 220 and 100 m2 g-1, respectively. TEM, BET and XRD results confirm that both crystal and pore sizes increase as a result of increasing the temperatures during the calcination step. This method is highly reproducible.",

keywords = "Mesoporous tin dioxide, TEM, BET , XRD, XPS, Pore and crystal sizes, Calcinations",

author = "Tariq Aqeel and Greer, \{Heather F.\} and Wuzong Zhou and Bruce, \{Duncan W.\} and Ali Bumajdad",

note = "This project is supported by PAAET project no. BE-‐13-‐08 in collaboration with Kuwait University and the University of York. The support of the research administration of Kuwait University to the XPS instrument (Project No. GS02/08) is acknowledged.",

year = "2016",

month = mar,

doi = "10.4028/www.scientific.net/JNanoR.40.79",

language = "English",

volume = "40",

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journal = "Journal of Nano Research",

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AU - Aqeel, Tariq

AU - Greer, Heather F.

AU - Zhou, Wuzong

AU - Bruce, Duncan W.

AU - Bumajdad, Ali

N1 - This project is supported by PAAET project no. BE-‐13-‐08 in collaboration with Kuwait University and the University of York. The support of the research administration of Kuwait University to the XPS instrument (Project No. GS02/08) is acknowledged.

PY - 2016/3

Y1 - 2016/3

N2 - We present a direct soft templating method to synthesise mesoporous tin dioxide network that maintains a porous structure after calcination at 400 °C and 500 °C and has a relatively high BET surface area of 220 and 100 m2 g-1, respectively. TEM, BET and XRD results confirm that both crystal and pore sizes increase as a result of increasing the temperatures during the calcination step. This method is highly reproducible.

AB - We present a direct soft templating method to synthesise mesoporous tin dioxide network that maintains a porous structure after calcination at 400 °C and 500 °C and has a relatively high BET surface area of 220 and 100 m2 g-1, respectively. TEM, BET and XRD results confirm that both crystal and pore sizes increase as a result of increasing the temperatures during the calcination step. This method is highly reproducible.

KW - Mesoporous tin dioxide

KW - TEM

KW - BET

KW - XRD

KW - XPS

KW - Pore and crystal sizes

KW - Calcinations

U2 - 10.4028/www.scientific.net/JNanoR.40.79

DO - 10.4028/www.scientific.net/JNanoR.40.79

M3 - Article

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SN - 1662-5250

VL - 40

SP - 79

EP - 89

JO - Journal of Nano Research

JF - Journal of Nano Research

ER -

Novel direct synthesis of mesoporous tin dioxide network intact up to 500°C

Abstract

Keywords

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Projects

Energy Materials Discovery: Energy Materials Discovery Characterisation and Application

EP/F019580/1 - Electron Microscopy: Electron Microscopy of Advanced Materials

Cite this