N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds

S M S V  Wardell; M V D R E  Silva; P F  Prado; J N  Low; C  Glidewell

doi:10.1107/S0108270104006109

N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds

S M S V Wardell, M V D R E Silva, P F Prado, J N Low, C Glidewell

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

Molecules of the title compound, C21H30N2O6S2, adopt a skeletal conformation which does not possess even approximate internal symmetry. The molecules are linked by two N-H...O=S hydrogen bonds [H...O=1.97 Angstrom (x2), N...O=2.865 (2) and 2.864 (2) Angstrom, and N-H...O=160 and 159degrees] into molecular ladders, alternatively described as chains of edge-fused R-2(2)(20) rings.

Original language	English
Number of pages	3
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	60
DOIs	https://doi.org/10.1107/S0108270104006109
Publication status	Published - May 2004

Keywords

POWDER DIFFRACTION DATA
PATTERNS

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Wardell, S. M. S. V., Silva, M. V. D. R. E., Prado, P. F., Low, J. N., & Glidewell, C. (2004). N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds. Acta Crystallographica Section C-Crystal Structure Communications, 60. https://doi.org/10.1107/S0108270104006109

@article{8daf85568a4c4a00ae85bc9e9bc90179,

title = "N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds",

abstract = "Molecules of the title compound, C21H30N2O6S2, adopt a skeletal conformation which does not possess even approximate internal symmetry. The molecules are linked by two N-H...O=S hydrogen bonds [H...O=1.97 Angstrom (x2), N...O=2.865 (2) and 2.864 (2) Angstrom, and N-H...O=160 and 159degrees] into molecular ladders, alternatively described as chains of edge-fused R-2(2)(20) rings.",

keywords = "POWDER DIFFRACTION DATA, PATTERNS",

author = "Wardell, \{S M S V\} and Silva, \{M V D R E\} and Prado, \{P F\} and Low, \{J N\} and C Glidewell",

year = "2004",

month = may,

doi = "10.1107/S0108270104006109",

language = "English",

volume = "60",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

}

Wardell, SMSV, Silva, MVDRE, Prado, PF, Low, JN & Glidewell, C 2004, 'N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds', Acta Crystallographica Section C-Crystal Structure Communications, vol. 60. https://doi.org/10.1107/S0108270104006109

N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds. / Wardell, S M S V ; Silva, M V D R E ; Prado, P F et al.
In: Acta Crystallographica Section C-Crystal Structure Communications, Vol. 60, 05.2004.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds

AU - Wardell, S M S V

AU - Silva, M V D R E

AU - Prado, P F

AU - Low, J N

AU - Glidewell, C

PY - 2004/5

Y1 - 2004/5

N2 - Molecules of the title compound, C21H30N2O6S2, adopt a skeletal conformation which does not possess even approximate internal symmetry. The molecules are linked by two N-H...O=S hydrogen bonds [H...O=1.97 Angstrom (x2), N...O=2.865 (2) and 2.864 (2) Angstrom, and N-H...O=160 and 159degrees] into molecular ladders, alternatively described as chains of edge-fused R-2(2)(20) rings.

AB - Molecules of the title compound, C21H30N2O6S2, adopt a skeletal conformation which does not possess even approximate internal symmetry. The molecules are linked by two N-H...O=S hydrogen bonds [H...O=1.97 Angstrom (x2), N...O=2.865 (2) and 2.864 (2) Angstrom, and N-H...O=160 and 159degrees] into molecular ladders, alternatively described as chains of edge-fused R-2(2)(20) rings.

KW - POWDER DIFFRACTION DATA

KW - PATTERNS

UR - https://www.scopus.com/pages/publications/2942672868

U2 - 10.1107/S0108270104006109

DO - 10.1107/S0108270104006109

M3 - Article

SN - 1600-5759

SN - 0108-2701

VL - 60

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -

Wardell SMSV, Silva MVDRE, Prado PF, Low JN, Glidewell C. N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds. Acta Crystallographica Section C-Crystal Structure Communications. 2004 May;60. doi: 10.1107/S0108270104006109

N,N '-Propylenedioxybis(2,4,6-tri-methylbenzenesulfonamide): molecules of unexpected conformation form a molecular ladder built from two independent N-H center dot center dot center dot O=S hydrogen bonds

Abstract

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