Natural abundance 33S NMR spectroscopy. The first spectra of several major compound types

Robert Alan Aitken; S Arumugam; STE Mesher; Frank Gordon Riddell

doi:10.1039/b109478e

Natural abundance ³³S NMR spectroscopy. The first spectra of several major compound types

Robert Alan Aitken, S Arumugam, STE Mesher, Frank Gordon Riddell

Research output: Contribution to journal › Article › peer-review

Abstract

Using a high field, high power instrument, S-33 NMR spectra have been obtained for several previously unobservable compound types including an aromatic isothiocyanate, a thiocyanate, a thiophenol, an alkyl aryl sulfide, a thiazole, a persulfate, a sulfinic acid and sulnate salts, a sulfonhydrazide and a sulfinyl halide. The range of data for sulfonyl fluorides and chlorides has also been extended considerably.

Original language	English
Pages (from-to)	225-226
Number of pages	2
Journal	Journal of Chemical Society, Perkin Transactions 2
Issue number	2
DOIs	https://doi.org/10.1039/b109478e
Publication status	Published - Jan 2002

Keywords

STABILIZED PHOSPHORUS YLIDES
FLASH VACUUM PYROLYSIS
REACTIVITY
EXTRUSION
CARBENES
SULFONES
SULFIDES
PH3P

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Cite this

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title = "Natural abundance 33S NMR spectroscopy. The first spectra of several major compound types",

abstract = "Using a high field, high power instrument, S-33 NMR spectra have been obtained for several previously unobservable compound types including an aromatic isothiocyanate, a thiocyanate, a thiophenol, an alkyl aryl sulfide, a thiazole, a persulfate, a sulfinic acid and sulnate salts, a sulfonhydrazide and a sulfinyl halide. The range of data for sulfonyl fluorides and chlorides has also been extended considerably.",

keywords = "STABILIZED PHOSPHORUS YLIDES, FLASH VACUUM PYROLYSIS, REACTIVITY, EXTRUSION, CARBENES, SULFONES, SULFIDES, PH3P",

author = "Aitken, \{Robert Alan\} and S Arumugam and STE Mesher and Riddell, \{Frank Gordon\}",

year = "2002",

month = jan,

doi = "10.1039/b109478e",

language = "English",

pages = "225--226",

journal = "Journal of Chemical Society, Perkin Transactions 2",

issn = "1472-779X",

publisher = "Royal Society of Chemistry",

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T1 - Natural abundance 33S NMR spectroscopy. The first spectra of several major compound types

AU - Aitken, Robert Alan

AU - Arumugam, S

AU - Mesher, STE

AU - Riddell, Frank Gordon

PY - 2002/1

Y1 - 2002/1

N2 - Using a high field, high power instrument, S-33 NMR spectra have been obtained for several previously unobservable compound types including an aromatic isothiocyanate, a thiocyanate, a thiophenol, an alkyl aryl sulfide, a thiazole, a persulfate, a sulfinic acid and sulnate salts, a sulfonhydrazide and a sulfinyl halide. The range of data for sulfonyl fluorides and chlorides has also been extended considerably.

AB - Using a high field, high power instrument, S-33 NMR spectra have been obtained for several previously unobservable compound types including an aromatic isothiocyanate, a thiocyanate, a thiophenol, an alkyl aryl sulfide, a thiazole, a persulfate, a sulfinic acid and sulnate salts, a sulfonhydrazide and a sulfinyl halide. The range of data for sulfonyl fluorides and chlorides has also been extended considerably.

KW - STABILIZED PHOSPHORUS YLIDES

KW - FLASH VACUUM PYROLYSIS

KW - REACTIVITY

KW - EXTRUSION

KW - CARBENES

KW - SULFONES

KW - SULFIDES

KW - PH3P

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UR - http://www.rsc.org/delivery/_ArticleLinking/DisplayArticleForFree.cfm?doi=b109478e&JournalCode=P2

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DO - 10.1039/b109478e

M3 - Article

SN - 1472-779X

SP - 225

EP - 226

JO - Journal of Chemical Society, Perkin Transactions 2

JF - Journal of Chemical Society, Perkin Transactions 2

IS - 2

ER -