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A study into the disassembly and organisation steps of the ADOR process has been undertaken through in situ Pair Distribution Function (PDF) analysis. Three aqueous systems (water, 6 M HCl and 12 M HCl) were introduced to a parent zeolite germanosilicate UTL in a cell. Hydrolysis could be clearly seen when UTL was exposed to water over a period of 8 hr, forming the disorded layered material, IPC-1P. In hydrochloric acid, the hydrolysis step is too quick to observe and a Ge-Cl containing species could be seen. In 6 M HCl, the rearrangement of the interlayer region began after an induction period of 8 hr, with the process still occuring after 15 hr. In 12 M HCl, the rearrangement appears to have come to an end after only 6 hr.
FingerprintDive into the research topics of 'Monitoring the assembly-disassembly-organisation-reassembly process of germanosilicate UTL through in situ pair distribution function analysis'. Together they form a unique fingerprint.
- 2 Finished
Assembly Disassembly Reassembly: Assembly disassembly reassembly - New routes to extended structures and their impact
1/08/13 → 31/07/18
1/03/13 → 28/02/16
Monitoring the Assembly-Disassembly-Organisation-Reassembly Process of Germanosilicate UTL through in situ Pair Distribution Function Analysis (dataset)