Methyl 4-amino-2,3-dihydro-6-methoxy-1,3-dioxo-1H-pyrrolo[3,4-c]-pyridine-7-carboxylate forms hydrogen-bonded sheets built from R-2(2)(8) and R-6(6)(42) rings

J N  Low; J  Cobo; C  Garcia; M  Melguizo; M  Nogueras; A  Sanchez; C  Glidewell

Methyl 4-amino-2,3-dihydro-6-methoxy-1,3-dioxo-1H-pyrrolo[3,4-c]-pyridine-7-carboxylate forms hydrogen-bonded sheets built from R-2(2)(8) and R-6(6)(42) rings

J N Low, J Cobo, C Garcia, M Melguizo, M Nogueras, A Sanchez, C Glidewell

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

In the title compound, C10H9N3O5, which was formed by the reaction of 6-amino-2-methoxy-4(3H)-pyrimidinone with dimethyl acetylenedicarboxylate, the molecules are linked by N-H . . . O hydrogen bonds [N . . . O 2.8974 (15) and 3.0300 (15) Angstrom , and N-H . . . O 165 and 174 degrees] into planar sheets built from alternating R-2(2)(8) and R-6(6)(42) rings.

Original language	English
Pages (from-to)	597-599
Number of pages	3
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	57
Publication status	Published - May 2001

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@article{f99d945dca2f4878aadc131bbfff01a6,

title = "Methyl 4-amino-2,3-dihydro-6-methoxy-1,3-dioxo-1H-pyrrolo[3,4-c]-pyridine-7-carboxylate forms hydrogen-bonded sheets built from R-2(2)(8) and R-6(6)(42) rings",

abstract = "In the title compound, C10H9N3O5, which was formed by the reaction of 6-amino-2-methoxy-4(3H)-pyrimidinone with dimethyl acetylenedicarboxylate, the molecules are linked by N-H . . . O hydrogen bonds [N . . . O 2.8974 (15) and 3.0300 (15) Angstrom , and N-H . . . O 165 and 174 degrees] into planar sheets built from alternating R-2(2)(8) and R-6(6)(42) rings.",

author = "Low, \{J N\} and J Cobo and C Garcia and M Melguizo and M Nogueras and A Sanchez and C Glidewell",

year = "2001",

month = may,

language = "English",

volume = "57",

pages = "597--599",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

}

TY - JOUR

T1 - Methyl 4-amino-2,3-dihydro-6-methoxy-1,3-dioxo-1H-pyrrolo[3,4-c]-pyridine-7-carboxylate forms hydrogen-bonded sheets built from R-2(2)(8) and R-6(6)(42) rings

AU - Low, J N

AU - Cobo, J

AU - Garcia, C

AU - Melguizo, M

AU - Nogueras, M

AU - Sanchez, A

AU - Glidewell, C

PY - 2001/5

Y1 - 2001/5

N2 - In the title compound, C10H9N3O5, which was formed by the reaction of 6-amino-2-methoxy-4(3H)-pyrimidinone with dimethyl acetylenedicarboxylate, the molecules are linked by N-H . . . O hydrogen bonds [N . . . O 2.8974 (15) and 3.0300 (15) Angstrom , and N-H . . . O 165 and 174 degrees] into planar sheets built from alternating R-2(2)(8) and R-6(6)(42) rings.

AB - In the title compound, C10H9N3O5, which was formed by the reaction of 6-amino-2-methoxy-4(3H)-pyrimidinone with dimethyl acetylenedicarboxylate, the molecules are linked by N-H . . . O hydrogen bonds [N . . . O 2.8974 (15) and 3.0300 (15) Angstrom , and N-H . . . O 165 and 174 degrees] into planar sheets built from alternating R-2(2)(8) and R-6(6)(42) rings.

M3 - Article

SN - 1600-5759

SN - 0108-2701

VL - 57

SP - 597

EP - 599

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -

Methyl 4-amino-2,3-dihydro-6-methoxy-1,3-dioxo-1H-pyrrolo[3,4-c]-pyridine-7-carboxylate forms hydrogen-bonded sheets built from R-2(2)(8) and R-6(6)(42) rings

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