meso-5,5,7,12,12,14-Hexamethyl-4,11-diaza-1,8-diazoniacyclotetradecane(S)-malate(2-)methanol disolvate: a chain of rings generated by two pairs of N-H center dot center dot center dot O hydrogen bonds

K F Bowes, G Ferguson, A J Lough, C Glidewell

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2 Citations (Scopus)

Abstract

The title compound is a methanol-solvated salt, C16H38N42+.C4H4O52-.2CH(3)OH, in which the ionic components are linked into chains by two pairs of N-H...O hydrogen bonds [H...O = 1.78 - 2.21 Angstrom, N...O = 2.702 (14) - 3.094 (8) Angstrom and N - H...O = 160 - 179 degrees]. The methanol molecules are pendent from the chain and are linked to it by O - H...O hydrogen bonds [H...O = 1.86 and 1.89 Angstrom, O...O = 2.691 (9) and 2.708 (16) Angstrom, and O - H...O = 168 and 165 degrees].

Original languageEnglish
Number of pages3
JournalActa Crystallographica Section C-Crystal Structure Communications
Volume59
DOIs
Publication statusPublished - Jun 2003

Keywords

  • RACEMIC BUILDING-BLOCKS
  • SUPRAMOLECULAR CHEMISTRY
  • ORGANIC DIAMINES
  • SALTS
  • DIMENSIONS
  • ADDUCTS
  • ACIDS

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