P,P,P′,P′-Tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate)

Jaden K. Jones; Aidan P. McKay; David Cordes; Brian Chalmers

doi:10.3390/M2104

P,P,P′,P′-Tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate)

Jaden K. Jones
, Aidan P. McKay
, David Cordes
, Brian Chalmers^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

We report the synthesis and molecular structure as determined by single-crystal X-ray diffraction of P,P,P′,P′-tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate). The compound was fully characterized by 1H, 13C, and 31P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.

Original language	English
Article number	M2104
Journal	Molbank
Volume	2025
Issue number	4
DOIs	https://doi.org/10.3390/M2104
Publication status	Published - 8 Dec 2025

Keywords

Pudovik reaction
X-ray crystallography
NMR spectroscopy
Bis(phosphonate)

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10.3390/M2104Licence: CC BY

Jones_2025_Molbank_P-P-P-P_CC
Copyright © 2025 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
Final published version, 1.08 MBLicence: CC BY

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title = "P,P,P′,P′-Tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate)",

abstract = "We report the synthesis and molecular structure as determined by single-crystal X-ray diffraction of P,P,P′,P′-tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate). The compound was fully characterized by 1H, 13C, and 31P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.",

keywords = "Pudovik reaction, X-ray crystallography, NMR spectroscopy, Bis(phosphonate)",

author = "Jones, \{Jaden K.\} and McKay, \{Aidan P.\} and David Cordes and Brian Chalmers",

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doi = "10.3390/M2104",

language = "English",

volume = "2025",

journal = "Molbank",

issn = "1422-8599",

publisher = "Multidisciplinary Digital Publishing Institute (MDPI)",

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TY - JOUR

T1 - P,P,P′,P′-Tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate)

AU - Jones, Jaden K.

AU - McKay, Aidan P.

AU - Cordes, David

AU - Chalmers, Brian

PY - 2025/12/8

Y1 - 2025/12/8

N2 - We report the synthesis and molecular structure as determined by single-crystal X-ray diffraction of P,P,P′,P′-tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate). The compound was fully characterized by 1H, 13C, and 31P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.

AB - We report the synthesis and molecular structure as determined by single-crystal X-ray diffraction of P,P,P′,P′-tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate). The compound was fully characterized by 1H, 13C, and 31P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.

KW - Pudovik reaction

KW - X-ray crystallography

KW - NMR spectroscopy

KW - Bis(phosphonate)

U2 - 10.3390/M2104

DO - 10.3390/M2104

M3 - Article

SN - 1422-8599

VL - 2025

JO - Molbank

JF - Molbank

IS - 4

M1 - M2104

ER -

P,P,P′,P′-Tetraisopropyl(1,4-phenylenebis(hydroxymethylene))bis(phosphonate)

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