Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1)

P S  Wheatley; A J  Lough; G  Ferguson; C  Glidewell

doi:10.1107/S0108270199006356

Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1)

P S Wheatley
, A J Lough
, G Ferguson
, C Glidewell

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

The 1:1 adduct of 5-hydroxyisophthalie acid and 4,4'-trimethylenedipyridine is a salt, [HNC5H4(CH2)(3)C5H4N](+).[HOC6H3(COOH)COO](-) (C13H15N2+. C8H5O5-). The anions are linked into C(7) chains by means of O-H ... O hydrogen bonds [O ... O 2.734 (2) Angstrom and O-H ... O 176 degrees], and these chains are linked by the cations via O-H ... N and N-H ... O hydrogen bonds [O ... N 2.620(2) Angstrom, O-H ... N 175 degrees, N ... O 2.748(2) Angstrom and N-H ... O 176 degrees] into four identical but independent interpenetrating three-dimensional frameworks.

Original language	English
Pages (from-to)	1486-1489
Number of pages	4
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	55
Issue number	9
DOIs	https://doi.org/10.1107/S0108270199006356
Publication status	Published - 15 Sept 1999

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@article{fa49d772af4743b5b1200a9e1ce9c2ef,

title = "Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1)",

abstract = "The 1:1 adduct of 5-hydroxyisophthalie acid and 4,4'-trimethylenedipyridine is a salt, [HNC5H4(CH2)(3)C5H4N](+).[HOC6H3(COOH)COO](-) (C13H15N2+. C8H5O5-). The anions are linked into C(7) chains by means of O-H ... O hydrogen bonds [O ... O 2.734 (2) Angstrom and O-H ... O 176 degrees], and these chains are linked by the cations via O-H ... N and N-H ... O hydrogen bonds [O ... N 2.620(2) Angstrom, O-H ... N 175 degrees, N ... O 2.748(2) Angstrom and N-H ... O 176 degrees] into four identical but independent interpenetrating three-dimensional frameworks.",

author = "Wheatley, \{P S\} and Lough, \{A J\} and G Ferguson and C Glidewell",

year = "1999",

month = sep,

day = "15",

doi = "10.1107/S0108270199006356",

language = "English",

volume = "55",

pages = "1486--1489",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

number = "9",

}

Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1). / Wheatley, P S ; Lough, A J ; Ferguson, G et al.
In: Acta Crystallographica Section C-Crystal Structure Communications, Vol. 55, No. 9, 15.09.1999, p. 1486-1489.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1)

AU - Wheatley, P S

AU - Lough, A J

AU - Ferguson, G

AU - Glidewell, C

PY - 1999/9/15

Y1 - 1999/9/15

N2 - The 1:1 adduct of 5-hydroxyisophthalie acid and 4,4'-trimethylenedipyridine is a salt, [HNC5H4(CH2)(3)C5H4N](+).[HOC6H3(COOH)COO](-) (C13H15N2+. C8H5O5-). The anions are linked into C(7) chains by means of O-H ... O hydrogen bonds [O ... O 2.734 (2) Angstrom and O-H ... O 176 degrees], and these chains are linked by the cations via O-H ... N and N-H ... O hydrogen bonds [O ... N 2.620(2) Angstrom, O-H ... N 175 degrees, N ... O 2.748(2) Angstrom and N-H ... O 176 degrees] into four identical but independent interpenetrating three-dimensional frameworks.

AB - The 1:1 adduct of 5-hydroxyisophthalie acid and 4,4'-trimethylenedipyridine is a salt, [HNC5H4(CH2)(3)C5H4N](+).[HOC6H3(COOH)COO](-) (C13H15N2+. C8H5O5-). The anions are linked into C(7) chains by means of O-H ... O hydrogen bonds [O ... O 2.734 (2) Angstrom and O-H ... O 176 degrees], and these chains are linked by the cations via O-H ... N and N-H ... O hydrogen bonds [O ... N 2.620(2) Angstrom, O-H ... N 175 degrees, N ... O 2.748(2) Angstrom and N-H ... O 176 degrees] into four identical but independent interpenetrating three-dimensional frameworks.

UR - https://www.scopus.com/pages/publications/0004363129

U2 - 10.1107/S0108270199006356

DO - 10.1107/S0108270199006356

M3 - Article

SN - 1600-5759

SN - 0108-2701

VL - 55

SP - 1486

EP - 1489

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

IS - 9

ER -

Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid-4,4 '-trimethylenedipyridine (1/1)

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