Ethyl (2RS,3SR,4RS)-1-ethyl-2-(furan-2-yl)-4-hydroxy-5-oxopyrrolidine-3- carboxylate

Nor Habibah Mohd  Rosli; Mohd Fazli  Mohammat; Mohd Abdul Fatah  Abdul Manan; David Bradford Cordes; Aidan McKay

doi:10.1107/S2414314624010885

Ethyl (2RS,3SR,4RS)-1-ethyl-2-(furan-2-yl)-4-hydroxy-5-oxopyrrolidine-3- carboxylate

Nor Habibah Mohd Rosli, Mohd Fazli Mohammat, Mohd Abdul Fatah Abdul Manan, David Bradford Cordes, Aidan McKay

Research output: Contribution to journal › Article › peer-review

Abstract

The title racemic oxopyrrolidine compound, C13H17NO5, contains three stereogenic centres and crystallized with two independent molecules in the asymmetric unit. The five-membered pyrrolidine ring in both molecules exhibit an envelope
conformation. In the crystal, independent molecules form dimers through O–H···O hydrogen bonds which then are linked together by weak C–H···O hydrogen bonds.

Original language	English
Journal	IUCrData
Volume	9
Issue number	11
DOIs	https://doi.org/10.1107/S2414314624010885
Publication status	Published - 19 Nov 2024

Keywords

crystal structure
oxopyrrolidine
racemic
envelope conformation
hydrogen bonds

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10.1107/S2414314624010885Licence: CC BY

Rosli_2024_IUCrData_Ethyl_CCBY
Copyright © 2024 The Authors. This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
Final published version, 2.45 MBLicence: CC BY

CCDC 2401488: Experimental Crystal Structure Determination
Rosli, N. H. M. (Creator), Mohammat, M. F. (Creator), Manan, M. A. F. A. (Creator), Cordes, D. B. (Creator) & McKay, A. P. (Creator), Cambridge Crystallographic Data Centre, 2024
DOI: 10.5517/ccdc.csd.cc2llycj
Dataset

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@article{d4995efdba8b48c5ab1483abb1bc37e5,

title = "Ethyl (2RS,3SR,4RS)-1-ethyl-2-(furan-2-yl)-4-hydroxy-5-oxopyrrolidine-3- carboxylate",

abstract = "The title racemic oxopyrrolidine compound, C13H17NO5, contains three stereogenic centres and crystallized with two independent molecules in the asymmetric unit. The five-membered pyrrolidine ring in both molecules exhibit an envelopeconformation. In the crystal, independent molecules form dimers through O–H···O hydrogen bonds which then are linked together by weak C–H···O hydrogen bonds.",

keywords = "crystal structure, oxopyrrolidine, racemic, envelope conformation, hydrogen bonds",

author = "Rosli, {Nor Habibah Mohd} and Mohammat, {Mohd Fazli} and {Abdul Manan}, {Mohd Abdul Fatah} and Cordes, {David Bradford} and Aidan McKay",

note = "Funding: The authors acknowledge Universiti Teknologi MARA for financial support.",

year = "2024",

month = nov,

day = "19",

doi = "10.1107/S2414314624010885",

language = "English",

volume = "9",

journal = "IUCrData",

issn = "2414-3146",

publisher = "International Union of Crystallography",

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TY - JOUR

T1 - Ethyl (2RS,3SR,4RS)-1-ethyl-2-(furan-2-yl)-4-hydroxy-5-oxopyrrolidine-3- carboxylate

AU - Rosli, Nor Habibah Mohd

AU - Mohammat, Mohd Fazli

AU - Abdul Manan, Mohd Abdul Fatah

AU - Cordes, David Bradford

AU - McKay, Aidan

N1 - Funding: The authors acknowledge Universiti Teknologi MARA for financial support.

PY - 2024/11/19

Y1 - 2024/11/19

N2 - The title racemic oxopyrrolidine compound, C13H17NO5, contains three stereogenic centres and crystallized with two independent molecules in the asymmetric unit. The five-membered pyrrolidine ring in both molecules exhibit an envelopeconformation. In the crystal, independent molecules form dimers through O–H···O hydrogen bonds which then are linked together by weak C–H···O hydrogen bonds.

AB - The title racemic oxopyrrolidine compound, C13H17NO5, contains three stereogenic centres and crystallized with two independent molecules in the asymmetric unit. The five-membered pyrrolidine ring in both molecules exhibit an envelopeconformation. In the crystal, independent molecules form dimers through O–H···O hydrogen bonds which then are linked together by weak C–H···O hydrogen bonds.

KW - crystal structure

KW - oxopyrrolidine

KW - racemic

KW - envelope conformation

KW - hydrogen bonds

U2 - 10.1107/S2414314624010885

DO - 10.1107/S2414314624010885

M3 - Article

SN - 2414-3146

VL - 9

JO - IUCrData

JF - IUCrData

IS - 11

ER -

Ethyl (2RS,3SR,4RS)-1-ethyl-2-(furan-2-yl)-4-hydroxy-5-oxopyrrolidine-3- carboxylate

Abstract

Keywords

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Datasets

CCDC 2401488: Experimental Crystal Structure Determination

Cite this