Diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate

Andy I. Coker; Aidan P. McKay; David B. Cordes; Brian A. Chalmers

doi:10.3390/M2013

Diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate

Andy I. Coker, Aidan P. McKay, David B. Cordes, Brian A. Chalmers^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

We report the synthesis and the molecular structure as determined by single-crystal X-ray diffraction of diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate. The compound was fully characterised by ¹H, ¹³C, and ³¹P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.

Original language	English
Article number	M2013
Number of pages	7
Journal	Molbank
Volume	2025
Issue number	2
Early online date	27 May 2025
DOIs	https://doi.org/10.3390/M2013
Publication status	Published - 1 Jun 2025

Keywords

NMR spectroscopy
Pudovik reaction
X-ray crystallography
α-hydroxyphosphonates

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10.3390/M2013Licence: CC BY

Coker_2025_Molbank_Diisopropyl-E-(1-hydroxy-3-phenylallyl)-phosphate_CC
© 2025 by the authors. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
Final published version, 717 KBLicence: CC BY

Cite this

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title = "Diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate",

abstract = "We report the synthesis and the molecular structure as determined by single-crystal X-ray diffraction of diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate. The compound was fully characterised by 1H, 13C, and 31P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.",

keywords = "NMR spectroscopy, Pudovik reaction, X-ray crystallography, α-hydroxyphosphonates",

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T1 - Diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate

AU - Coker, Andy I.

AU - McKay, Aidan P.

AU - Cordes, David B.

AU - Chalmers, Brian A.

PY - 2025/6/1

Y1 - 2025/6/1

N2 - We report the synthesis and the molecular structure as determined by single-crystal X-ray diffraction of diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate. The compound was fully characterised by 1H, 13C, and 31P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.

AB - We report the synthesis and the molecular structure as determined by single-crystal X-ray diffraction of diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate. The compound was fully characterised by 1H, 13C, and 31P NMR spectroscopy, IR spectroscopy, and Mass Spectrometry.

KW - NMR spectroscopy

KW - Pudovik reaction

KW - X-ray crystallography

KW - α-hydroxyphosphonates

UR - https://www.scopus.com/pages/publications/105009256532

U2 - 10.3390/M2013

DO - 10.3390/M2013

M3 - Article

AN - SCOPUS:105009256532

SN - 1422-8599

VL - 2025

JO - Molbank

JF - Molbank

IS - 2

M1 - M2013

ER -

Diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate

Abstract

Keywords

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CCDC 2443736: Experimental Crystal Structure Determination

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Diisopropyl (E)-(1-hydroxy-3-phenylallyl)phosphonate

Abstract

Keywords

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Datasets

CCDC 2443736: Experimental Crystal Structure Determination

Cite this