Bis(4-hydroxybenzoato-O)(1,4,8,11-tetraazacyclotetradecane-kappa N-4)-nickel(II): a three-dimensional framework built from O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds

C  Glidewell; G  Ferguson; R M  Gregson; A J  Lough

Bis(4-hydroxybenzoato-O)(1,4,8,11-tetraazacyclotetradecane-kappa N-4)-nickel(II): a three-dimensional framework built from O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds

C Glidewell, G Ferguson, R M Gregson, A J Lough

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

The title compound, [Ni(C7H5O3)(2)(C10H24N4)], contains octahedral Ni-II in a centrosymmetric trans configuration with Ni-N distances of 2.0637 (17) and 2.0699 (16) Angstrom and an Ni-O distance of 2.1100 (14) Angstrom. The molecules are linked by a single type of O-H ... O hydrogen bond [O ... O 2.618 (2) Angstrom and O-H ... O 161 degrees] into two-dimensional sheets; a single type of N-H ... O hydrogen bond [N ... O 2.991 (2) Angstrom and N-H ... O 139 degrees] links these sheets into a three-dimensional framework.

Original language	English
Pages (from-to)	174-176
Number of pages	3
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	56
Publication status	Published - Feb 2000

Keywords

CRYSTAL-STRUCTURE
COMPLEXES
1,4,8,11-TETRAAZACYCLOTETRADECANE
CYCLAM

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Glidewell, C ; Ferguson, G ; Gregson, R M et al. / Bis(4-hydroxybenzoato-O)(1,4,8,11-tetraazacyclotetradecane-kappa N-4)-nickel(II): a three-dimensional framework built from O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds. In: Acta Crystallographica Section C-Crystal Structure Communications. 2000 ; Vol. 56. pp. 174-176.

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title = "Bis(4-hydroxybenzoato-O)(1,4,8,11-tetraazacyclotetradecane-kappa N-4)-nickel(II): a three-dimensional framework built from O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds",

abstract = "The title compound, [Ni(C7H5O3)(2)(C10H24N4)], contains octahedral Ni-II in a centrosymmetric trans configuration with Ni-N distances of 2.0637 (17) and 2.0699 (16) Angstrom and an Ni-O distance of 2.1100 (14) Angstrom. The molecules are linked by a single type of O-H ... O hydrogen bond [O ... O 2.618 (2) Angstrom and O-H ... O 161 degrees] into two-dimensional sheets; a single type of N-H ... O hydrogen bond [N ... O 2.991 (2) Angstrom and N-H ... O 139 degrees] links these sheets into a three-dimensional framework.",

keywords = "CRYSTAL-STRUCTURE, COMPLEXES, 1,4,8,11-TETRAAZACYCLOTETRADECANE, CYCLAM",

author = "C Glidewell and G Ferguson and Gregson, {R M} and Lough, {A J}",

year = "2000",

month = feb,

language = "English",

volume = "56",

pages = "174--176",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

}

Bis(4-hydroxybenzoato-O)(1,4,8,11-tetraazacyclotetradecane-kappa N-4)-nickel(II): a three-dimensional framework built from O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds. / Glidewell, C ; Ferguson, G ; Gregson, R M et al.
In: Acta Crystallographica Section C-Crystal Structure Communications, Vol. 56, 02.2000, p. 174-176.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Bis(4-hydroxybenzoato-O)(1,4,8,11-tetraazacyclotetradecane-kappa N-4)-nickel(II): a three-dimensional framework built from O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds

AU - Glidewell, C

AU - Ferguson, G

AU - Gregson, R M

AU - Lough, A J

PY - 2000/2

Y1 - 2000/2

N2 - The title compound, [Ni(C7H5O3)(2)(C10H24N4)], contains octahedral Ni-II in a centrosymmetric trans configuration with Ni-N distances of 2.0637 (17) and 2.0699 (16) Angstrom and an Ni-O distance of 2.1100 (14) Angstrom. The molecules are linked by a single type of O-H ... O hydrogen bond [O ... O 2.618 (2) Angstrom and O-H ... O 161 degrees] into two-dimensional sheets; a single type of N-H ... O hydrogen bond [N ... O 2.991 (2) Angstrom and N-H ... O 139 degrees] links these sheets into a three-dimensional framework.

AB - The title compound, [Ni(C7H5O3)(2)(C10H24N4)], contains octahedral Ni-II in a centrosymmetric trans configuration with Ni-N distances of 2.0637 (17) and 2.0699 (16) Angstrom and an Ni-O distance of 2.1100 (14) Angstrom. The molecules are linked by a single type of O-H ... O hydrogen bond [O ... O 2.618 (2) Angstrom and O-H ... O 161 degrees] into two-dimensional sheets; a single type of N-H ... O hydrogen bond [N ... O 2.991 (2) Angstrom and N-H ... O 139 degrees] links these sheets into a three-dimensional framework.

KW - CRYSTAL-STRUCTURE

KW - COMPLEXES

KW - 1,4,8,11-TETRAAZACYCLOTETRADECANE

KW - CYCLAM

M3 - Article

SN - 1600-5759

VL - 56

SP - 174

EP - 176

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -