Benzo[d][1,2,3]oxadithiole 2-oxide

R Alan Aitken; David Bradford Cordes; Arun Goyal; Aidan McKay

doi:10.3390/M1803

Benzo[d][1,2,3]oxadithiole 2-oxide

R Alan Aitken^*, David Bradford Cordes, Arun Goyal, Aidan McKay

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

A simplified synthesis of the title compound is reported and its ¹H and ¹³C NMR data are fully assigned including determination of H–H and C–H coupling constants. Its X-ray structure has been determined for the first time. NMR data are also presented for the oxygen analogue.

Original language	English
Article number	M1803
Number of pages	6
Journal	Molbank
Volume	2024
Issue number	2
DOIs	https://doi.org/10.3390/M1803
Publication status	Published - 7 Apr 2024

Keywords

X-ray structure
NMR spectra

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10.3390/M1803Licence: CC BY

Aitken-2024-Benzo-Molbank-2024-M1803-CCBY
Copyright: © 2024 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https:// creativecommons.org/licenses/by/4.0/).
Final published version, 2.37 MBLicence: CC BY

Cite this

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title = "Benzo[d][1,2,3]oxadithiole 2-oxide",

abstract = "A simplified synthesis of the title compound is reported and its 1H and 13C NMR data are fully assigned including determination of H–H and C–H coupling constants. Its X-ray structure has been determined for the first time. NMR data are also presented for the oxygen analogue.",

keywords = "X-ray structure, NMR spectra",

author = "Aitken, {R Alan} and Cordes, {David Bradford} and Arun Goyal and Aidan McKay",

note = "Funding: A.G. thanks the Commissionerate of College Education, Government of Rajasthan for the generous support of a Foreign Training Program under its Teachers' Interface for Excellence Scheme. ",

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AU - Aitken, R Alan

AU - Cordes, David Bradford

AU - Goyal, Arun

AU - McKay, Aidan

N1 - Funding: A.G. thanks the Commissionerate of College Education, Government of Rajasthan for the generous support of a Foreign Training Program under its Teachers' Interface for Excellence Scheme.

PY - 2024/4/7

Y1 - 2024/4/7

N2 - A simplified synthesis of the title compound is reported and its 1H and 13C NMR data are fully assigned including determination of H–H and C–H coupling constants. Its X-ray structure has been determined for the first time. NMR data are also presented for the oxygen analogue.

AB - A simplified synthesis of the title compound is reported and its 1H and 13C NMR data are fully assigned including determination of H–H and C–H coupling constants. Its X-ray structure has been determined for the first time. NMR data are also presented for the oxygen analogue.

KW - X-ray structure

KW - NMR spectra

UR - https://www.mdpi.com/1422-8599/2024/2/M1803

U2 - 10.3390/M1803

DO - 10.3390/M1803

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SN - 1422-8599

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ER -

Benzo[d][1,2,3]oxadithiole 2-oxide

Abstract

Keywords

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CCDC 2340013: Experimental Crystal Structure Determination

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Benzo[d][1,2,3]oxadithiole 2-oxide

Abstract

Keywords

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Datasets

CCDC 2340013: Experimental Crystal Structure Determination

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