Ammonium oxathioamidate

M. Carla Aragoni, David Bradford Cordes, Anna Pintus, Enrico Podda, Riccardo Serra, Alexandra Martha Zoya Slawin, J Derek Woollins, Massimiliano Arca*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

Abstract

Ammonium oxathioamidate (1) was synthesized by the reaction between O-ethyl-thioxamate (oxalic acid-1-amide-2-O-ethyl ester) and ammonium hydrogen carbonate in water solution. Compound 1 was fully characterized by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by slow evaporation of an ethanol solution of the compound. The analysis of the crystal packing reveals the prominent role exerted by intermolecular hydrogen bonding (HB) and chalcogen bonding (ChB) interactions.
Original languageEnglish
Article numberM1924
Number of pages7
JournalMolbank
Volume2024
Issue number4
DOIs
Publication statusPublished - 26 Nov 2024

Keywords

  • Thiooxamate
  • Oxalic acid derivatives
  • Hydrogen bonding
  • XRD

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