Abstract
Ammonium oxathioamidate (1) was synthesized by the reaction between O-ethyl-thioxamate (oxalic acid-1-amide-2-O-ethyl ester) and ammonium hydrogen carbonate in water solution. Compound 1 was fully characterized by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by slow evaporation of an ethanol solution of the compound. The analysis of the crystal packing reveals the prominent role exerted by intermolecular hydrogen bonding (HB) and chalcogen bonding (ChB) interactions.
Original language | English |
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Article number | M1924 |
Number of pages | 7 |
Journal | Molbank |
Volume | 2024 |
Issue number | 4 |
DOIs | |
Publication status | Published - 26 Nov 2024 |
Keywords
- Thiooxamate
- Oxalic acid derivatives
- Hydrogen bonding
- XRD
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CCDC 2391872: Experimental Crystal Structure Determination
Aragoni, M. C. (Creator), Cordes (Creator), Pintus, A. (Creator), Podda, E. (Creator), Riccardo, S. (Creator), Slawin (Creator), Derek, J. (Creator) & Arca, M. (Creator), Cambridge Crystallographic Data Centre, 2024
DOI: 10.5517/ccdc.csd.cc2l8y50
Dataset