Ammonium N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl) glycinate monohydrate forms hydrogen-bonded bilayers

P A  Mascaros; R C  Martos; C  Glidewell; J N  Low

doi:10.1107/S0108270103009181

Ammonium N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl) glycinate monohydrate forms hydrogen-bonded bilayers

P A Mascaros, R C Martos, C Glidewell, J N Low

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

In the title compound, NH4+.C7H8N5O4-.H2O, the independent components are linked into bilayers by an extensive series of two-centre N-H...O hydrogen bonds [H...O = 1.85 - 1.96 Angstrom, N...O = 2.776 (2) - 2.840 (2) Angstrom and N - H...O = 149 - 172 degrees], and by asymmetric three-centre N - H ...(O)(2), O - H ...(N, O) and O - H ...(O)(2) hydrogen bonds.

Original language	English
Number of pages	3
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	59
DOIs	https://doi.org/10.1107/S0108270103009181
Publication status	Published - Jun 2003

Keywords

SUPRAMOLECULAR STRUCTURES

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title = "Ammonium N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl) glycinate monohydrate forms hydrogen-bonded bilayers",

abstract = "In the title compound, NH4+.C7H8N5O4-.H2O, the independent components are linked into bilayers by an extensive series of two-centre N-H...O hydrogen bonds [H...O = 1.85 - 1.96 Angstrom, N...O = 2.776 (2) - 2.840 (2) Angstrom and N - H...O = 149 - 172 degrees], and by asymmetric three-centre N - H ...(O)(2), O - H ...(N, O) and O - H ...(O)(2) hydrogen bonds.",

keywords = "SUPRAMOLECULAR STRUCTURES",

author = "Mascaros, {P A} and Martos, {R C} and C Glidewell and Low, {J N}",

year = "2003",

month = jun,

doi = "10.1107/S0108270103009181",

language = "English",

volume = "59",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

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TY - JOUR

T1 - Ammonium N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl) glycinate monohydrate forms hydrogen-bonded bilayers

AU - Mascaros, P A

AU - Martos, R C

AU - Glidewell, C

AU - Low, J N

PY - 2003/6

Y1 - 2003/6

N2 - In the title compound, NH4+.C7H8N5O4-.H2O, the independent components are linked into bilayers by an extensive series of two-centre N-H...O hydrogen bonds [H...O = 1.85 - 1.96 Angstrom, N...O = 2.776 (2) - 2.840 (2) Angstrom and N - H...O = 149 - 172 degrees], and by asymmetric three-centre N - H ...(O)(2), O - H ...(N, O) and O - H ...(O)(2) hydrogen bonds.

AB - In the title compound, NH4+.C7H8N5O4-.H2O, the independent components are linked into bilayers by an extensive series of two-centre N-H...O hydrogen bonds [H...O = 1.85 - 1.96 Angstrom, N...O = 2.776 (2) - 2.840 (2) Angstrom and N - H...O = 149 - 172 degrees], and by asymmetric three-centre N - H ...(O)(2), O - H ...(N, O) and O - H ...(O)(2) hydrogen bonds.

KW - SUPRAMOLECULAR STRUCTURES

U2 - 10.1107/S0108270103009181

DO - 10.1107/S0108270103009181

M3 - Article

SN - 1600-5759

VL - 59

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -

Ammonium N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl) glycinate monohydrate forms hydrogen-bonded bilayers

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