A three-dimensional hydrogen-bonded framework in piperazine-3,4-dihydroxy3-cyclobutene-1,2-dione-water (1/1/2)

E J  MacLean; P S  Wheatley; G  Ferguson; C  Glidewell; A J  Lough

doi:10.1107/S0108270199009531

A three-dimensional hydrogen-bonded framework in piperazine-3,4-dihydroxy3-cyclobutene-1,2-dione-water (1/1/2)

E J MacLean
, P S Wheatley
, G Ferguson
, C Glidewell
, A J Lough

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

The title compound, piperazine-1,4-diium 3,4-dihydroxy-3-cyclobutene- 1,2-dionate(2-) dihydrate, is a hydrated salt, C4H12N22+. C4O42-. 2H(2)O The water molecules and the centrosymmetric anions are linked by O-H ... O hydrogen bonds into two-dimensional nets built from a single type of R-8(6)(24) ring. Adjacent nets are linked by the centrosymmetric cations, each of which forms four N-H ... O hydrogen bonds, with four different anions as accepters.

Original language	English
Pages (from-to)	1896-1899
Number of pages	4
Journal	Acta Crystallographica Section C: Crystal Structure Communications
Volume	55
Issue number	11
DOIs	https://doi.org/10.1107/S0108270199009531
Publication status	Published - 15 Nov 1999

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title = "A three-dimensional hydrogen-bonded framework in piperazine-3,4-dihydroxy3-cyclobutene-1,2-dione-water (1/1/2)",

abstract = "The title compound, piperazine-1,4-diium 3,4-dihydroxy-3-cyclobutene- 1,2-dionate(2-) dihydrate, is a hydrated salt, C4H12N22+. C4O42-. 2H(2)O The water molecules and the centrosymmetric anions are linked by O-H ... O hydrogen bonds into two-dimensional nets built from a single type of R-8(6)(24) ring. Adjacent nets are linked by the centrosymmetric cations, each of which forms four N-H ... O hydrogen bonds, with four different anions as accepters.",

author = "MacLean, \{E J\} and Wheatley, \{P S\} and G Ferguson and C Glidewell and Lough, \{A J\}",

year = "1999",

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doi = "10.1107/S0108270199009531",

language = "English",

volume = "55",

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publisher = "International Union of Crystallography",

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TY - JOUR

T1 - A three-dimensional hydrogen-bonded framework in piperazine-3,4-dihydroxy3-cyclobutene-1,2-dione-water (1/1/2)

AU - MacLean, E J

AU - Wheatley, P S

AU - Ferguson, G

AU - Glidewell, C

AU - Lough, A J

PY - 1999/11/15

Y1 - 1999/11/15

N2 - The title compound, piperazine-1,4-diium 3,4-dihydroxy-3-cyclobutene- 1,2-dionate(2-) dihydrate, is a hydrated salt, C4H12N22+. C4O42-. 2H(2)O The water molecules and the centrosymmetric anions are linked by O-H ... O hydrogen bonds into two-dimensional nets built from a single type of R-8(6)(24) ring. Adjacent nets are linked by the centrosymmetric cations, each of which forms four N-H ... O hydrogen bonds, with four different anions as accepters.

AB - The title compound, piperazine-1,4-diium 3,4-dihydroxy-3-cyclobutene- 1,2-dionate(2-) dihydrate, is a hydrated salt, C4H12N22+. C4O42-. 2H(2)O The water molecules and the centrosymmetric anions are linked by O-H ... O hydrogen bonds into two-dimensional nets built from a single type of R-8(6)(24) ring. Adjacent nets are linked by the centrosymmetric cations, each of which forms four N-H ... O hydrogen bonds, with four different anions as accepters.

UR - https://www.scopus.com/pages/publications/0008785026

U2 - 10.1107/S0108270199009531

DO - 10.1107/S0108270199009531

M3 - Article

SN - 0108-2701

VL - 55

SP - 1896

EP - 1899

JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

IS - 11

ER -

A three-dimensional hydrogen-bonded framework in piperazine-3,4-dihydroxy3-cyclobutene-1,2-dione-water (1/1/2)

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