A synthesis, MAS NMR, synchrotron X-ray powder diffraction, and computational study of zeolite SSZ-23

MA Camblor; M-J Díaz-Cabañas; PA Cos; IJ Shannon; Paul Anthony Wright; Russell Edward Morris

A synthesis, MAS NMR, synchrotron X-ray powder diffraction, and computational study of zeolite SSZ-23

MA Camblor, M-J Díaz-Cabañas, PA Cos, IJ Shannon, Paul Anthony Wright, Russell Edward Morris

Research output: Contribution to journal › Article › peer-review

Abstract

The zeolite SSZ-23 (STT) is the first zeolite found to contain channels bounded by seven and nine tetrahedral atom windows. A survey of the synthetic conditions needed to prepare SSZ-23 has been carried out, and the resulting materials characterized by synchrotron X-ray powder diffraction and magic-angle spinning NMR spectroscopy to obtain details of the long-range crystalline structure and short-range connectivity defects. The lattice energy minimized structure is in excellent agreement with the experimental results, and a comparison with other zeolites that have been simulated in this way is made.

Original language	English
Pages (from-to)	2878-2885
Number of pages	8
Journal	Chemistry of Materials
Volume	11
Publication status	Published - Oct 1999

Keywords

SPECTROSCOPY

Cite this

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title = "A synthesis, MAS NMR, synchrotron X-ray powder diffraction, and computational study of zeolite SSZ-23",

abstract = "The zeolite SSZ-23 (STT) is the first zeolite found to contain channels bounded by seven and nine tetrahedral atom windows. A survey of the synthetic conditions needed to prepare SSZ-23 has been carried out, and the resulting materials characterized by synchrotron X-ray powder diffraction and magic-angle spinning NMR spectroscopy to obtain details of the long-range crystalline structure and short-range connectivity defects. The lattice energy minimized structure is in excellent agreement with the experimental results, and a comparison with other zeolites that have been simulated in this way is made.",

keywords = "SPECTROSCOPY",

author = "MA Camblor and M-J D{\'i}az-Caba{\~n}as and PA Cos and IJ Shannon and Wright, \{Paul Anthony\} and Morris, \{Russell Edward\}",

year = "1999",

month = oct,

language = "English",

volume = "11",

pages = "2878--2885",

journal = "Chemistry of Materials",

issn = "0897-4756",

publisher = "American Chemical Society (ACS)",

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TY - JOUR

T1 - A synthesis, MAS NMR, synchrotron X-ray powder diffraction, and computational study of zeolite SSZ-23

AU - Camblor, MA

AU - Díaz-Cabañas, M-J

AU - Cos, PA

AU - Shannon, IJ

AU - Wright, Paul Anthony

AU - Morris, Russell Edward

PY - 1999/10

Y1 - 1999/10

N2 - The zeolite SSZ-23 (STT) is the first zeolite found to contain channels bounded by seven and nine tetrahedral atom windows. A survey of the synthetic conditions needed to prepare SSZ-23 has been carried out, and the resulting materials characterized by synchrotron X-ray powder diffraction and magic-angle spinning NMR spectroscopy to obtain details of the long-range crystalline structure and short-range connectivity defects. The lattice energy minimized structure is in excellent agreement with the experimental results, and a comparison with other zeolites that have been simulated in this way is made.

AB - The zeolite SSZ-23 (STT) is the first zeolite found to contain channels bounded by seven and nine tetrahedral atom windows. A survey of the synthetic conditions needed to prepare SSZ-23 has been carried out, and the resulting materials characterized by synchrotron X-ray powder diffraction and magic-angle spinning NMR spectroscopy to obtain details of the long-range crystalline structure and short-range connectivity defects. The lattice energy minimized structure is in excellent agreement with the experimental results, and a comparison with other zeolites that have been simulated in this way is made.

KW - SPECTROSCOPY

UR - https://www.scopus.com/pages/publications/0003786279

M3 - Article

SN - 0897-4756

VL - 11

SP - 2878

EP - 2885

JO - Chemistry of Materials

JF - Chemistry of Materials

ER -

A synthesis, MAS NMR, synchrotron X-ray powder diffraction, and computational study of zeolite SSZ-23

Abstract

Keywords

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