A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices

Abhra Giri; Subir K. Patla; Madhumita Mukhopadhyay; Jayanta Mukhopadhyay; Monalisa Mukherjee; Ruma Ray; Sujata Tarafdar

doi:10.1007/978-981-33-6915-3_30

A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices

Abhra Giri, Subir K. Patla, Madhumita Mukhopadhyay^*, Jayanta Mukhopadhyay, Monalisa Mukherjee, Ruma Ray, Sujata Tarafdar

^*Corresponding author for this work

School of Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

Porous polymer films of Poly-[Ethylene oxide] (PEO) are synthesized by solution casting technique using gamma irradiated: (a) PEO powder (S-series) and (b) PEO—methanol solution (L-series). Pore phase is though a defect, but form instantaneously during preparation. Optimization of the pore content, its size and distribution enable tailoring of associated properties for multifaceted applications of functional materials. The experimental pore-size distribution of the PEO films is studied using BET (Brunauer–Emmet–Teller) adsorption technique and reported as function of irradiation dose, irradiation state (S- and L-series) and polymer concentration (2 and 4 wt%). A newer computer program [PROG_IMAGE-POR] is reported for determination of porosity, its size and distribution of perturbed PEO films using SEM images and correlated with that obtained from BET technique. The novelty of PROG_IMAGE-POR lies in the exposure of newer or undetected pore regime in which experimental pore regime exists as a part. This method could be analyzed for mapping of porosity and average pore size. PROG_IMAGE-POR bears the novelty of using image from either 2D or 3D imaging system and could be applied for intricate composite/layered system. Uniqueness of PROG_IMAGE-POR lies in the exposure of newer pore regime in which experimental pores exist as a part. Theoretical analysis based on aerosity (2D-pores) and porosity (3D-pore) gives an estimate of the tortuous path of void space.

Original language	English
Title of host publication	Advances in Medical Physics and Healthcare Engineering
Subtitle of host publication	Proceedings of AMPHE 2020
Editors	Moumita Mukherjee, J. K. Mandal, Siddhartha Bhattacharyya, Christian Huck, Satarupa Biswas
Place of Publication	Singapore
Publisher	Springer Nature Singapore
Pages	289-310
Number of pages	22
ISBN (Electronic)	9789813369153
ISBN (Print)	9789813369146
DOIs	https://doi.org/10.1007/978-981-33-6915-3_30
Publication status	Published - 17 Jun 2021
Event	Advances in Medical Physics and Healthcare Engineering 2020 - Adamas University, Kolkata, India Duration: 25 Sept 2020 → 26 Sept 2020 https://science.adamasuniversity.ac.in/amphe2020/#1568796496215-a9ad091c-7baa

Publication series

Name	Lecture Notes in Bioengineering
ISSN (Print)	2195-271X
ISSN (Electronic)	2195-2728

Conference

Conference	Advances in Medical Physics and Healthcare Engineering 2020
Abbreviated title	AMPHE 2020
Country/Territory	India
City	Kolkata
Period	25/09/20 → 26/09/20
Internet address	https://science.adamasuniversity.ac.in/amphe2020/#1568796496215-a9ad091c-7baa

Keywords

Porosity
Morphology
Pore-size distribution
Computer program
Gray-scale pixel
Gamma irradiation

Access to Document

10.1007/978-981-33-6915-3_30

Cite this

Giri, A., Patla, S. K., Mukhopadhyay, M., Mukhopadhyay, J., Mukherjee, M., Ray, R., & Tarafdar, S. (2021). A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices. In M. Mukherjee, J. K. Mandal, S. Bhattacharyya, C. Huck, & S. Biswas (Eds.), Advances in Medical Physics and Healthcare Engineering: Proceedings of AMPHE 2020 (pp. 289-310). (Lecture Notes in Bioengineering). Springer Nature Singapore. https://doi.org/10.1007/978-981-33-6915-3_30

Giri, Abhra ; Patla, Subir K. ; Mukhopadhyay, Madhumita et al. / A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity : case studies using polymeric films and functional matrices. Advances in Medical Physics and Healthcare Engineering: Proceedings of AMPHE 2020. editor / Moumita Mukherjee ; J. K. Mandal ; Siddhartha Bhattacharyya ; Christian Huck ; Satarupa Biswas. Singapore : Springer Nature Singapore, 2021. pp. 289-310 (Lecture Notes in Bioengineering).

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title = "A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices",

abstract = "Porous polymer films of Poly-[Ethylene oxide] (PEO) are synthesized by solution casting technique using gamma irradiated: (a) PEO powder (S-series) and (b) PEO—methanol solution (L-series). Pore phase is though a defect, but form instantaneously during preparation. Optimization of the pore content, its size and distribution enable tailoring of associated properties for multifaceted applications of functional materials. The experimental pore-size distribution of the PEO films is studied using BET (Brunauer–Emmet–Teller) adsorption technique and reported as function of irradiation dose, irradiation state (S- and L-series) and polymer concentration (2 and 4 wt%). A newer computer program [PROGIMAGE-POR] is reported for determination of porosity, its size and distribution of perturbed PEO films using SEM images and correlated with that obtained from BET technique. The novelty of PROGIMAGE-POR lies in the exposure of newer or undetected pore regime in which experimental pore regime exists as a part. This method could be analyzed for mapping of porosity and average pore size. PROGIMAGE-POR bears the novelty of using image from either 2D or 3D imaging system and could be applied for intricate composite/layered system. Uniqueness of PROGIMAGE-POR lies in the exposure of newer pore regime in which experimental pores exist as a part. Theoretical analysis based on aerosity (2D-pores) and porosity (3D-pore) gives an estimate of the tortuous path of void space.",

keywords = "Porosity, Morphology, Pore-size distribution, Computer program, Gray-scale pixel, Gamma irradiation",

author = "Abhra Giri and Patla, {Subir K.} and Madhumita Mukhopadhyay and Jayanta Mukhopadhyay and Monalisa Mukherjee and Ruma Ray and Sujata Tarafdar",

note = "Funding: The Corresponding author MM acknowledges Amity University, Kolkata, for infrastructural support. SKP is thankful to Inter-University Accelerator Centre (IUAC), Delhi, for providing Junior Research fellowship. Dr. Paramita Bhattacharyya and Miss. Suchisrawa Ghosh of Department of Food Technology, Jadavpur University, Kolkata, are acknowledged for extending their support in using the gamma irradiation chamber. The Authors also acknowledge FIST-2, DST Government of India, at the Physics Department, Jadavpur University, for providing the facility of SEM microscope. JM acknowledges Director, CSIR- CGCRI for kind permission to present the work. Dr. Monalisa Mukherjee acknowledges AIBN, AICCRS, Amity University, Noida, for necessary support.; Advances in Medical Physics and Healthcare Engineering 2020, AMPHE 2020 ; Conference date: 25-09-2020 Through 26-09-2020",

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month = jun,

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doi = "10.1007/978-981-33-6915-3_30",

language = "English",

isbn = "9789813369146",

series = "Lecture Notes in Bioengineering",

publisher = "Springer Nature Singapore",

pages = "289--310",

editor = "Moumita Mukherjee and Mandal, {J. K.} and Siddhartha Bhattacharyya and Christian Huck and Satarupa Biswas",

booktitle = "Advances in Medical Physics and Healthcare Engineering",

url = "https://science.adamasuniversity.ac.in/amphe2020/#1568796496215-a9ad091c-7baa",

}

Giri, A, Patla, SK, Mukhopadhyay, M, Mukhopadhyay, J, Mukherjee, M, Ray, R & Tarafdar, S 2021, A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices. in M Mukherjee, JK Mandal, S Bhattacharyya, C Huck & S Biswas (eds), Advances in Medical Physics and Healthcare Engineering: Proceedings of AMPHE 2020. Lecture Notes in Bioengineering, Springer Nature Singapore, Singapore, pp. 289-310, Advances in Medical Physics and Healthcare Engineering 2020, Kolkata, India, 25/09/20. https://doi.org/10.1007/978-981-33-6915-3_30

A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices. / Giri, Abhra; Patla, Subir K.; Mukhopadhyay, Madhumita et al.
Advances in Medical Physics and Healthcare Engineering: Proceedings of AMPHE 2020. ed. / Moumita Mukherjee; J. K. Mandal; Siddhartha Bhattacharyya; Christian Huck; Satarupa Biswas. Singapore: Springer Nature Singapore, 2021. p. 289-310 (Lecture Notes in Bioengineering).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

TY - GEN

T1 - A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity

T2 - Advances in Medical Physics and Healthcare Engineering 2020

AU - Giri, Abhra

AU - Patla, Subir K.

AU - Mukhopadhyay, Madhumita

AU - Mukhopadhyay, Jayanta

AU - Mukherjee, Monalisa

AU - Ray, Ruma

AU - Tarafdar, Sujata

N1 - Funding: The Corresponding author MM acknowledges Amity University, Kolkata, for infrastructural support. SKP is thankful to Inter-University Accelerator Centre (IUAC), Delhi, for providing Junior Research fellowship. Dr. Paramita Bhattacharyya and Miss. Suchisrawa Ghosh of Department of Food Technology, Jadavpur University, Kolkata, are acknowledged for extending their support in using the gamma irradiation chamber. The Authors also acknowledge FIST-2, DST Government of India, at the Physics Department, Jadavpur University, for providing the facility of SEM microscope. JM acknowledges Director, CSIR- CGCRI for kind permission to present the work. Dr. Monalisa Mukherjee acknowledges AIBN, AICCRS, Amity University, Noida, for necessary support.

PY - 2021/6/17

Y1 - 2021/6/17

N2 - Porous polymer films of Poly-[Ethylene oxide] (PEO) are synthesized by solution casting technique using gamma irradiated: (a) PEO powder (S-series) and (b) PEO—methanol solution (L-series). Pore phase is though a defect, but form instantaneously during preparation. Optimization of the pore content, its size and distribution enable tailoring of associated properties for multifaceted applications of functional materials. The experimental pore-size distribution of the PEO films is studied using BET (Brunauer–Emmet–Teller) adsorption technique and reported as function of irradiation dose, irradiation state (S- and L-series) and polymer concentration (2 and 4 wt%). A newer computer program [PROGIMAGE-POR] is reported for determination of porosity, its size and distribution of perturbed PEO films using SEM images and correlated with that obtained from BET technique. The novelty of PROGIMAGE-POR lies in the exposure of newer or undetected pore regime in which experimental pore regime exists as a part. This method could be analyzed for mapping of porosity and average pore size. PROGIMAGE-POR bears the novelty of using image from either 2D or 3D imaging system and could be applied for intricate composite/layered system. Uniqueness of PROGIMAGE-POR lies in the exposure of newer pore regime in which experimental pores exist as a part. Theoretical analysis based on aerosity (2D-pores) and porosity (3D-pore) gives an estimate of the tortuous path of void space.

AB - Porous polymer films of Poly-[Ethylene oxide] (PEO) are synthesized by solution casting technique using gamma irradiated: (a) PEO powder (S-series) and (b) PEO—methanol solution (L-series). Pore phase is though a defect, but form instantaneously during preparation. Optimization of the pore content, its size and distribution enable tailoring of associated properties for multifaceted applications of functional materials. The experimental pore-size distribution of the PEO films is studied using BET (Brunauer–Emmet–Teller) adsorption technique and reported as function of irradiation dose, irradiation state (S- and L-series) and polymer concentration (2 and 4 wt%). A newer computer program [PROGIMAGE-POR] is reported for determination of porosity, its size and distribution of perturbed PEO films using SEM images and correlated with that obtained from BET technique. The novelty of PROGIMAGE-POR lies in the exposure of newer or undetected pore regime in which experimental pore regime exists as a part. This method could be analyzed for mapping of porosity and average pore size. PROGIMAGE-POR bears the novelty of using image from either 2D or 3D imaging system and could be applied for intricate composite/layered system. Uniqueness of PROGIMAGE-POR lies in the exposure of newer pore regime in which experimental pores exist as a part. Theoretical analysis based on aerosity (2D-pores) and porosity (3D-pore) gives an estimate of the tortuous path of void space.

KW - Porosity

KW - Morphology

KW - Pore-size distribution

KW - Computer program

KW - Gray-scale pixel

KW - Gamma irradiation

U2 - 10.1007/978-981-33-6915-3_30

DO - 10.1007/978-981-33-6915-3_30

M3 - Conference contribution

AN - SCOPUS:85111827210

SN - 9789813369146

T3 - Lecture Notes in Bioengineering

SP - 289

EP - 310

BT - Advances in Medical Physics and Healthcare Engineering

A2 - Mukherjee, Moumita

A2 - Mandal, J. K.

A2 - Bhattacharyya, Siddhartha

A2 - Huck, Christian

A2 - Biswas, Satarupa

PB - Springer Nature Singapore

CY - Singapore

Y2 - 25 September 2020 through 26 September 2020

ER -

Giri A, Patla SK, Mukhopadhyay M, Mukhopadhyay J, Mukherjee M, Ray R et al. A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices. In Mukherjee M, Mandal JK, Bhattacharyya S, Huck C, Biswas S, editors, Advances in Medical Physics and Healthcare Engineering: Proceedings of AMPHE 2020. Singapore: Springer Nature Singapore. 2021. p. 289-310. (Lecture Notes in Bioengineering). doi: 10.1007/978-981-33-6915-3_30

A new approach of using microscopic image aided computer programming for evaluation of porosity and aerosity: case studies using polymeric films and functional matrices

Abstract

Publication series

Conference

Keywords

Access to Document

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