8-Bromonaphthalen-1-amine

Amy L. Fuller; Fergus R. Knight; Alexandra M. Z. Slawin; J. Derek Woollins

doi:10.1107/S1600536808012580

8-Bromonaphthalen-1-amine

Amy L. Fuller
, Fergus R. Knight
, Alexandra M. Z. Slawin
, J. Derek Woollins

Research output: Contribution to journal › Article › peer-review

Abstract

The title compound, C10H8BrN, was obtained by slow addition of sodium azide to 8-bromo-1-naphthoic acid, followed by addition of aqueous ammonia. The crude product was crystallized from petroleum ether to give pink crystals. Compared to other 1,8-disubstituted naphthalene compounds, this compound exhibits less strain between the 1 and 8 substituents. Additionally, the NH protons form both intra- and intermolecular hydrogen bonds. The naphthalene units are arranged in a herring-bone stacking motif.

Original language	English
Number of pages	9
Journal	Acta Crystallographica. Section E, Structure reports online
Volume	64
DOIs	https://doi.org/10.1107/S1600536808012580
Publication status	Published - Jun 2008

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title = "8-Bromonaphthalen-1-amine",

abstract = "The title compound, C10H8BrN, was obtained by slow addition of sodium azide to 8-bromo-1-naphthoic acid, followed by addition of aqueous ammonia. The crude product was crystallized from petroleum ether to give pink crystals. Compared to other 1,8-disubstituted naphthalene compounds, this compound exhibits less strain between the 1 and 8 substituents. Additionally, the NH protons form both intra- and intermolecular hydrogen bonds. The naphthalene units are arranged in a herring-bone stacking motif.",

author = "Fuller, \{Amy L.\} and Knight, \{Fergus R.\} and Slawin, \{Alexandra M. Z.\} and Woollins, \{J. Derek\}",

year = "2008",

month = jun,

doi = "10.1107/S1600536808012580",

language = "English",

volume = "64",

journal = "Acta Crystallographica. Section E, Structure reports online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

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T1 - 8-Bromonaphthalen-1-amine

AU - Fuller, Amy L.

AU - Knight, Fergus R.

AU - Slawin, Alexandra M. Z.

AU - Woollins, J. Derek

PY - 2008/6

Y1 - 2008/6

N2 - The title compound, C10H8BrN, was obtained by slow addition of sodium azide to 8-bromo-1-naphthoic acid, followed by addition of aqueous ammonia. The crude product was crystallized from petroleum ether to give pink crystals. Compared to other 1,8-disubstituted naphthalene compounds, this compound exhibits less strain between the 1 and 8 substituents. Additionally, the NH protons form both intra- and intermolecular hydrogen bonds. The naphthalene units are arranged in a herring-bone stacking motif.

AB - The title compound, C10H8BrN, was obtained by slow addition of sodium azide to 8-bromo-1-naphthoic acid, followed by addition of aqueous ammonia. The crude product was crystallized from petroleum ether to give pink crystals. Compared to other 1,8-disubstituted naphthalene compounds, this compound exhibits less strain between the 1 and 8 substituents. Additionally, the NH protons form both intra- and intermolecular hydrogen bonds. The naphthalene units are arranged in a herring-bone stacking motif.

UR - https://www.scopus.com/pages/publications/57349196397

U2 - 10.1107/S1600536808012580

DO - 10.1107/S1600536808012580

M3 - Article

SN - 1600-5368

VL - 64

JO - Acta Crystallographica. Section E, Structure reports online

JF - Acta Crystallographica. Section E, Structure reports online

ER -

8-Bromonaphthalen-1-amine

Abstract

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