5-amino-3-tert-butyl-1-(4-nitrophenyl)-lH-pyrazole forms hydrogen-bonded sheets of alternating R-2(2)(20) andR(6)(6)(32) rings

J N  Low; J  Cobo; R  Abonia; J  Quiroga; C  Glidewell

doi:10.1107/S0108270104000678

5-amino-3-tert-butyl-1-(4-nitrophenyl)-lH-pyrazole forms hydrogen-bonded sheets of alternating R-2(2)(20) andR(6)(6)(32) rings

J N Low, J Cobo, R Abonia, J Quiroga, C Glidewell

School of Chemistry

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

Molecules of the title compound, C13H16N4O2, are linked by one N-H...O hydrogen bond [H...O = 2.47 degrees, N...O = 3.326 (2) Angstrom and N-H...O = 166degrees] and one N-H...N hydrogen bond [H...N = 2.19 Angstrom, N...N = 3.063 (2) Angstrom and N-H...N = 173degrees] into sheets containing alternating R-2(2)(20) and R-6(6)(32) rings, both types of which are centrosymmetric.

Original language	English
Number of pages	2
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	60
DOIs	https://doi.org/10.1107/S0108270104000678
Publication status	Published - Mar 2004

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title = "5-amino-3-tert-butyl-1-(4-nitrophenyl)-lH-pyrazole forms hydrogen-bonded sheets of alternating R-2(2)(20) andR(6)(6)(32) rings",

abstract = "Molecules of the title compound, C13H16N4O2, are linked by one N-H...O hydrogen bond [H...O = 2.47 degrees, N...O = 3.326 (2) Angstrom and N-H...O = 166degrees] and one N-H...N hydrogen bond [H...N = 2.19 Angstrom, N...N = 3.063 (2) Angstrom and N-H...N = 173degrees] into sheets containing alternating R-2(2)(20) and R-6(6)(32) rings, both types of which are centrosymmetric.",

author = "Low, {J N} and J Cobo and R Abonia and J Quiroga and C Glidewell",

year = "2004",

month = mar,

doi = "10.1107/S0108270104000678",

language = "English",

volume = "60",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

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TY - JOUR

T1 - 5-amino-3-tert-butyl-1-(4-nitrophenyl)-lH-pyrazole forms hydrogen-bonded sheets of alternating R-2(2)(20) andR(6)(6)(32) rings

AU - Low, J N

AU - Cobo, J

AU - Abonia, R

AU - Quiroga, J

AU - Glidewell, C

PY - 2004/3

Y1 - 2004/3

N2 - Molecules of the title compound, C13H16N4O2, are linked by one N-H...O hydrogen bond [H...O = 2.47 degrees, N...O = 3.326 (2) Angstrom and N-H...O = 166degrees] and one N-H...N hydrogen bond [H...N = 2.19 Angstrom, N...N = 3.063 (2) Angstrom and N-H...N = 173degrees] into sheets containing alternating R-2(2)(20) and R-6(6)(32) rings, both types of which are centrosymmetric.

AB - Molecules of the title compound, C13H16N4O2, are linked by one N-H...O hydrogen bond [H...O = 2.47 degrees, N...O = 3.326 (2) Angstrom and N-H...O = 166degrees] and one N-H...N hydrogen bond [H...N = 2.19 Angstrom, N...N = 3.063 (2) Angstrom and N-H...N = 173degrees] into sheets containing alternating R-2(2)(20) and R-6(6)(32) rings, both types of which are centrosymmetric.

U2 - 10.1107/S0108270104000678

DO - 10.1107/S0108270104000678

M3 - Article

SN - 1600-5759

VL - 60

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -

5-amino-3-tert-butyl-1-(4-nitrophenyl)-lH-pyrazole forms hydrogen-bonded sheets of alternating R-2(2)(20) andR(6)(6)(32) rings

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