5-Amino-3-methyl-1,2,4-thiadiazole

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Abstract

An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules
Original languageEnglish
Article numberM977
Number of pages5
JournalMolbank
Volume2018
Issue number1
DOIs
Publication statusPublished - 21 Jan 2018

Keywords

  • 1,2,4-thiadiazole
  • X-ray structure
  • IR spectrum
  • NMR spectra

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