5-Amino-3-methyl-1,2,4-thiadiazole

R. Alan Aitken; Alexandra M. Z. Slawin

doi:10.3390/M977

5-Amino-3-methyl-1,2,4-thiadiazole

R. Alan Aitken, Alexandra M. Z. Slawin

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Abstract

An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its ¹H and ¹³C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules

Original language	English
Article number	M977
Number of pages	5
Journal	Molbank
Volume	2018
Issue number	1
DOIs	https://doi.org/10.3390/M977
Publication status	Published - 21 Jan 2018

Keywords

1,2,4-thiadiazole
X-ray structure
IR spectrum
NMR spectra

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10.3390/M977Licence: CC BY

molbank-2018-M977
© 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
Final published version, 1.27 MBLicence: CC BY
molbank-2018-M977_SIFinal published version, 1.57 MBLicence: CC BY

Cite this

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title = "5-Amino-3-methyl-1,2,4-thiadiazole",

abstract = "An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules",

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AU - Aitken, R. Alan

AU - Slawin, Alexandra M. Z.

PY - 2018/1/21

Y1 - 2018/1/21

N2 - An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules

AB - An improved procedure for isolation of 5-amino-3-methyl-1,2,4-thiadiazole in pure form on a multi-gram scale without chromatography is reported. Its 1H and 13C NMR and IR data are presented and previously published erroneous data corrected. The molecular structure is confirmed by X-ray diffraction which shows layers consisting of an elaborate two-dimensional hydrogen bonded network of molecules

KW - 1,2,4-thiadiazole

KW - X-ray structure

KW - IR spectrum

KW - NMR spectra

UR - http://www.mdpi.com/1422-8599/2018/1/M977#supplementary

U2 - 10.3390/M977

DO - 10.3390/M977

M3 - Article

SN - 1422-8599

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JO - Molbank

JF - Molbank

IS - 1

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ER -

5-Amino-3-methyl-1,2,4-thiadiazole

Abstract

Keywords

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