4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds

K F  Bowes; G  Ferguson; A J  Lough; C  Glidewell

doi:10.1107/S0108270103011818

4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds

K F Bowes, G Ferguson, A J Lough, C Glidewell

School of Chemistry

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Abstract

In the title compound, C13H16N22+.2C(2)H(4)O(5)P(-), the cation lies across a twofold rotation axis in space group Fdd2. The anions are linked into molecular ladders by two O-H...O hydrogen bonds [H...O = 1.73 and 1.77 Angstrom, O...O = 2.538 (2) and 2.598 (3) Angstrom, and O-H...O = 160 and 170degrees], these ladders are linked into sheets by a single type of N-H...O hydrogen bond [H...O = 1.75 Angstrom, N...O = 2.624 (3) Angstrom and N-H...O = 171degrees] and the sheets are linked into a three-dimensional framework by a single type of C-H...O hydrogen bond [H...O = 2.48 Angstrom, C...O = 3.419 (4) Angstrom and C-H...O = 167degrees].

Original language	English
Number of pages	3
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	59
DOIs	https://doi.org/10.1107/S0108270103011818
Publication status	Published - Aug 2003

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Bowes, K. F., Ferguson, G., Lough, A. J., & Glidewell, C. (2003). 4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds. Acta Crystallographica Section C-Crystal Structure Communications, 59. https://doi.org/10.1107/S0108270103011818

Bowes, K F ; Ferguson, G ; Lough, A J et al. / 4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds. In: Acta Crystallographica Section C-Crystal Structure Communications. 2003 ; Vol. 59.

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title = "4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds",

abstract = "In the title compound, C13H16N22+.2C(2)H(4)O(5)P(-), the cation lies across a twofold rotation axis in space group Fdd2. The anions are linked into molecular ladders by two O-H...O hydrogen bonds [H...O = 1.73 and 1.77 Angstrom, O...O = 2.538 (2) and 2.598 (3) Angstrom, and O-H...O = 160 and 170degrees], these ladders are linked into sheets by a single type of N-H...O hydrogen bond [H...O = 1.75 Angstrom, N...O = 2.624 (3) Angstrom and N-H...O = 171degrees] and the sheets are linked into a three-dimensional framework by a single type of C-H...O hydrogen bond [H...O = 2.48 Angstrom, C...O = 3.419 (4) Angstrom and C-H...O = 167degrees].",

author = "Bowes, \{K F\} and G Ferguson and Lough, \{A J\} and C Glidewell",

year = "2003",

month = aug,

doi = "10.1107/S0108270103011818",

language = "English",

volume = "59",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

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Bowes, KF, Ferguson, G, Lough, AJ & Glidewell, C 2003, '4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds', Acta Crystallographica Section C-Crystal Structure Communications, vol. 59. https://doi.org/10.1107/S0108270103011818

4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds. / Bowes, K F ; Ferguson, G ; Lough, A J et al.
In: Acta Crystallographica Section C-Crystal Structure Communications, Vol. 59, 08.2003.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - 4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds

AU - Bowes, K F

AU - Ferguson, G

AU - Lough, A J

AU - Glidewell, C

PY - 2003/8

Y1 - 2003/8

N2 - In the title compound, C13H16N22+.2C(2)H(4)O(5)P(-), the cation lies across a twofold rotation axis in space group Fdd2. The anions are linked into molecular ladders by two O-H...O hydrogen bonds [H...O = 1.73 and 1.77 Angstrom, O...O = 2.538 (2) and 2.598 (3) Angstrom, and O-H...O = 160 and 170degrees], these ladders are linked into sheets by a single type of N-H...O hydrogen bond [H...O = 1.75 Angstrom, N...O = 2.624 (3) Angstrom and N-H...O = 171degrees] and the sheets are linked into a three-dimensional framework by a single type of C-H...O hydrogen bond [H...O = 2.48 Angstrom, C...O = 3.419 (4) Angstrom and C-H...O = 167degrees].

AB - In the title compound, C13H16N22+.2C(2)H(4)O(5)P(-), the cation lies across a twofold rotation axis in space group Fdd2. The anions are linked into molecular ladders by two O-H...O hydrogen bonds [H...O = 1.73 and 1.77 Angstrom, O...O = 2.538 (2) and 2.598 (3) Angstrom, and O-H...O = 160 and 170degrees], these ladders are linked into sheets by a single type of N-H...O hydrogen bond [H...O = 1.75 Angstrom, N...O = 2.624 (3) Angstrom and N-H...O = 171degrees] and the sheets are linked into a three-dimensional framework by a single type of C-H...O hydrogen bond [H...O = 2.48 Angstrom, C...O = 3.419 (4) Angstrom and C-H...O = 167degrees].

UR - https://www.scopus.com/pages/publications/0041363217

U2 - 10.1107/S0108270103011818

DO - 10.1107/S0108270103011818

M3 - Article

SN - 1600-5759

SN - 0108-2701

VL - 59

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -

Bowes KF, Ferguson G, Lough AJ, Glidewell C. 4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds. Acta Crystallographica Section C-Crystal Structure Communications. 2003 Aug;59. doi: 10.1107/S0108270103011818

4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds

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