TY - JOUR
T1 - 4,4 '-trimethylenedipyridinium bis[carboxymethylphosphonate(1-)]: a three-dimensional framework structure built from O - H center dot center dot center dot O, N - H center dot center dot center dot O and C - H center dot center dot center dot O hydrogen bonds
AU - Bowes, K F
AU - Ferguson, G
AU - Lough, A J
AU - Glidewell, C
PY - 2003/8
Y1 - 2003/8
N2 - In the title compound, C13H16N22+.2C(2)H(4)O(5)P(-), the cation lies across a twofold rotation axis in space group Fdd2. The anions are linked into molecular ladders by two O-H...O hydrogen bonds [H...O = 1.73 and 1.77 Angstrom, O...O = 2.538 (2) and 2.598 (3) Angstrom, and O-H...O = 160 and 170degrees], these ladders are linked into sheets by a single type of N-H...O hydrogen bond [H...O = 1.75 Angstrom, N...O = 2.624 (3) Angstrom and N-H...O = 171degrees] and the sheets are linked into a three-dimensional framework by a single type of C-H...O hydrogen bond [H...O = 2.48 Angstrom, C...O = 3.419 (4) Angstrom and C-H...O = 167degrees].
AB - In the title compound, C13H16N22+.2C(2)H(4)O(5)P(-), the cation lies across a twofold rotation axis in space group Fdd2. The anions are linked into molecular ladders by two O-H...O hydrogen bonds [H...O = 1.73 and 1.77 Angstrom, O...O = 2.538 (2) and 2.598 (3) Angstrom, and O-H...O = 160 and 170degrees], these ladders are linked into sheets by a single type of N-H...O hydrogen bond [H...O = 1.75 Angstrom, N...O = 2.624 (3) Angstrom and N-H...O = 171degrees] and the sheets are linked into a three-dimensional framework by a single type of C-H...O hydrogen bond [H...O = 2.48 Angstrom, C...O = 3.419 (4) Angstrom and C-H...O = 167degrees].
U2 - 10.1107/S0108270103011818
DO - 10.1107/S0108270103011818
M3 - Article
SN - 1600-5759
VL - 59
JO - Acta Crystallographica Section C-Crystal Structure Communications
JF - Acta Crystallographica Section C-Crystal Structure Communications
ER -