TY - JOUR
T1 - 4-iodoanilinium 3-nitrophthalate(1-): tripartite sheets built from O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds
AU - Glidewell, C
AU - Low, J N
AU - Skakle, J M S
AU - Wardell, J L
PY - 2003/9
Y1 - 2003/9
N2 - In the title compound, 4-iodoanilinium 2-carboxy-6-nitrobenzoate, C6H7IN+.C8H4NO6-, the anions are linked by an O-H...O hydrogen bond [H...O = 1.78 Angstrom, O...O = 2.614 (3) Angstrom and O-H...O = 171degrees] into C(7) chains, and these chains are linked by two two-centre N-H...O hydrogen bonds [H...O = 1.86 and 1.92 Angstrom, N...O = 2.700 (3) and 2.786 (3) Angstrom, and N-H...O = 153 and 158degrees] and one three-centre N-H...(O)(2) hydrogen bond [H...O = 2.02 and 2.41 Angstrom, N...O = 2.896 (3) and 2.789 (3) Angstrom, N-H...O = 162 and 105degrees, and O...H...O = 92degrees], thus forming sheets containing R-2(2)( 6), R-4(2)(8), R-3(3)(13) and R-4(4)(18) rings.
AB - In the title compound, 4-iodoanilinium 2-carboxy-6-nitrobenzoate, C6H7IN+.C8H4NO6-, the anions are linked by an O-H...O hydrogen bond [H...O = 1.78 Angstrom, O...O = 2.614 (3) Angstrom and O-H...O = 171degrees] into C(7) chains, and these chains are linked by two two-centre N-H...O hydrogen bonds [H...O = 1.86 and 1.92 Angstrom, N...O = 2.700 (3) and 2.786 (3) Angstrom, and N-H...O = 153 and 158degrees] and one three-centre N-H...(O)(2) hydrogen bond [H...O = 2.02 and 2.41 Angstrom, N...O = 2.896 (3) and 2.789 (3) Angstrom, N-H...O = 162 and 105degrees, and O...H...O = 92degrees], thus forming sheets containing R-2(2)( 6), R-4(2)(8), R-3(3)(13) and R-4(4)(18) rings.
KW - CRYSTALS
KW - RADII
U2 - 10.1107/S0108270103014434
DO - 10.1107/S0108270103014434
M3 - Article
SN - 1600-5759
VL - 59
JO - Acta Crystallographica Section C-Crystal Structure Communications
JF - Acta Crystallographica Section C-Crystal Structure Communications
ER -