2,6-exo-8,10-exo-4-Butyl-9-oxa-4-azatetracyclo[5.3.1.02,6.08,10]undecane-3,5-dione

R Alan Aitken; Fiona M. Fotherby; Alexandra M. Z. Slawin

doi:10.3390/M1320

2,6-exo-8,10-exo-4-Butyl-9-oxa-4-azatetracyclo[5.3.1.0^2,6.0^8,10]undecane-3,5-dione

R Alan Aitken^*
, Fiona M. Fotherby
, Alexandra M. Z. Slawin

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

The title epoxide was obtained by spontaneous epoxidation of the corresponding unsaturated imide in air or by peracid oxidation. Unambiguous assignment of the ¹H and ¹³C NMR spectra is achieved by comparison between analogous compounds and its X-ray structure confirms the exo,exo-configuration.

Original language	English
Article number	M1320
Number of pages	7
Journal	Molbank
Volume	2022
Issue number	1
DOIs	https://doi.org/10.3390/M1320
Publication status	Published - 20 Jan 2022

Keywords

Epoxide
Cyclic imide
X-ray structure
NMR assignment

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10.3390/M1320Licence: CC BY

molbank-2022-M1320
Copyright: © 2022 by the authors. Licensee MDPI, Basel, Switzerland. This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Final published version, 1.6 MBLicence: CC BY

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CCDC 2128556: Experimental Crystal Structure Determination
Aitken, R. A. (Creator), Fotherby, F. M. (Creator) & Slawin, A. M. Z. (Creator), Cambridge Crystallographic Data Centre, 2022
DOI: 10.5517/ccdc.csd.cc29fy3t
Dataset

Synthesis, structure and properties of some new dihydrotetrathiafulvalenes
Fotherby, F. M. (Author), Aitken, R. A. (Supervisor), 13 Jun 2024
Student thesis: Doctoral Thesis (PhD)

Cite this

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title = "2,6-exo-8,10-exo-4-Butyl-9-oxa-4-azatetracyclo[5.3.1.02,6.08,10]undecane-3,5-dione",

abstract = "The title epoxide was obtained by spontaneous epoxidation of the corresponding unsaturated imide in air or by peracid oxidation. Unambiguous assignment of the 1H and 13C NMR spectra is achieved by comparison between analogous compounds and its X-ray structure confirms the exo,exo-configuration.",

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AU - Aitken, R Alan

AU - Fotherby, Fiona M.

AU - Slawin, Alexandra M. Z.

PY - 2022/1/20

Y1 - 2022/1/20

N2 - The title epoxide was obtained by spontaneous epoxidation of the corresponding unsaturated imide in air or by peracid oxidation. Unambiguous assignment of the 1H and 13C NMR spectra is achieved by comparison between analogous compounds and its X-ray structure confirms the exo,exo-configuration.

AB - The title epoxide was obtained by spontaneous epoxidation of the corresponding unsaturated imide in air or by peracid oxidation. Unambiguous assignment of the 1H and 13C NMR spectra is achieved by comparison between analogous compounds and its X-ray structure confirms the exo,exo-configuration.

KW - Epoxide

KW - Cyclic imide

KW - X-ray structure

KW - NMR assignment

U2 - 10.3390/M1320

DO - 10.3390/M1320

M3 - Article

SN - 1422-8599

VL - 2022

JO - Molbank

JF - Molbank

IS - 1

M1 - M1320

ER -

2,6-exo-8,10-exo-4-Butyl-9-oxa-4-azatetracyclo[5.3.1.02,6.08,10]undecane-3,5-dione

Abstract

Keywords

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Datasets

CCDC 2128556: Experimental Crystal Structure Determination

Student theses

Synthesis, structure and properties of some new dihydrotetrathiafulvalenes

Cite this

2,6-exo-8,10-exo-4-Butyl-9-oxa-4-azatetracyclo[5.3.1.0^2,6.0^8,10]undecane-3,5-dione