2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions

Monica A. Peralta; Marcus N. V. de Souza; Solange M. S. V. Wardell; James L. Wardell; John N. Low; Christopher Glidewell

doi:10.1107/S0108270106052486

2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions

Monica A. Peralta, Marcus N. V. de Souza, Solange M. S. V. Wardell, James L. Wardell, John N. Low, Christopher Glidewell

School of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

In 2,3-dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, C15H15N3O3 center dot CHCl3, the hydrazone molecules are linked by a combination of N-H center dot center dot center dot N and C-H center dot center dot center dot N hydrogen bonds into chains from which the chloroform molecules are pendent. 3,4,5-Trimethoxybenzaldehyde isonicotinoylhydrazone forms two stoichiometric hydrates. In the monohydrate, C16H17N3O4 center dot H2O, the components are linked into sheets by a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot N hydrogen bonds, and in the dihydrate, C16H17N3O4 center dot 2H(2)O, a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot O hydrogen bonds links the components into a three-dimensional framework structure.

Original language	English
Number of pages	5
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	63
DOIs	https://doi.org/10.1107/S0108270106052486
Publication status	Published - Jan 2007

Keywords

CRYSTAL-STRUCTURE
HYDRAZONE

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Peralta, M. A., de Souza, M. N. V., Wardell, S. M. S. V., Wardell, J. L., Low, J. N., & Glidewell, C. (2007). 2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions. Acta Crystallographica Section C-Crystal Structure Communications, 63. https://doi.org/10.1107/S0108270106052486

Peralta, Monica A. ; de Souza, Marcus N. V. ; Wardell, Solange M. S. V. et al. / 2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions. In: Acta Crystallographica Section C-Crystal Structure Communications. 2007 ; Vol. 63.

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title = "2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions",

abstract = "In 2,3-dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, C15H15N3O3 center dot CHCl3, the hydrazone molecules are linked by a combination of N-H center dot center dot center dot N and C-H center dot center dot center dot N hydrogen bonds into chains from which the chloroform molecules are pendent. 3,4,5-Trimethoxybenzaldehyde isonicotinoylhydrazone forms two stoichiometric hydrates. In the monohydrate, C16H17N3O4 center dot H2O, the components are linked into sheets by a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot N hydrogen bonds, and in the dihydrate, C16H17N3O4 center dot 2H(2)O, a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot O hydrogen bonds links the components into a three-dimensional framework structure.",

keywords = "CRYSTAL-STRUCTURE, HYDRAZONE",

author = "Peralta, {Monica A.} and {de Souza}, {Marcus N. V.} and Wardell, {Solange M. S. V.} and Wardell, {James L.} and Low, {John N.} and Christopher Glidewell",

year = "2007",

month = jan,

doi = "10.1107/S0108270106052486",

language = "English",

volume = "63",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

issn = "1600-5759",

publisher = "International Union of Crystallography",

}

Peralta, MA, de Souza, MNV, Wardell, SMSV, Wardell, JL, Low, JN & Glidewell, C 2007, '2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions', Acta Crystallographica Section C-Crystal Structure Communications, vol. 63. https://doi.org/10.1107/S0108270106052486

2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions. / Peralta, Monica A.; de Souza, Marcus N. V.; Wardell, Solange M. S. V. et al.
In: Acta Crystallographica Section C-Crystal Structure Communications, Vol. 63, 01.2007.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - 2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions

AU - Peralta, Monica A.

AU - de Souza, Marcus N. V.

AU - Wardell, Solange M. S. V.

AU - Wardell, James L.

AU - Low, John N.

AU - Glidewell, Christopher

PY - 2007/1

Y1 - 2007/1

N2 - In 2,3-dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, C15H15N3O3 center dot CHCl3, the hydrazone molecules are linked by a combination of N-H center dot center dot center dot N and C-H center dot center dot center dot N hydrogen bonds into chains from which the chloroform molecules are pendent. 3,4,5-Trimethoxybenzaldehyde isonicotinoylhydrazone forms two stoichiometric hydrates. In the monohydrate, C16H17N3O4 center dot H2O, the components are linked into sheets by a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot N hydrogen bonds, and in the dihydrate, C16H17N3O4 center dot 2H(2)O, a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot O hydrogen bonds links the components into a three-dimensional framework structure.

AB - In 2,3-dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, C15H15N3O3 center dot CHCl3, the hydrazone molecules are linked by a combination of N-H center dot center dot center dot N and C-H center dot center dot center dot N hydrogen bonds into chains from which the chloroform molecules are pendent. 3,4,5-Trimethoxybenzaldehyde isonicotinoylhydrazone forms two stoichiometric hydrates. In the monohydrate, C16H17N3O4 center dot H2O, the components are linked into sheets by a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot N hydrogen bonds, and in the dihydrate, C16H17N3O4 center dot 2H(2)O, a combination of O-H center dot center dot center dot O, O-H center dot center dot center dot N and N-H center dot center dot center dot O hydrogen bonds links the components into a three-dimensional framework structure.

KW - CRYSTAL-STRUCTURE

KW - HYDRAZONE

U2 - 10.1107/S0108270106052486

DO - 10.1107/S0108270106052486

M3 - Article

SN - 1600-5759

VL - 63

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -

Peralta MA, de Souza MNV, Wardell SMSV, Wardell JL, Low JN, Glidewell C. 2,3-Dimethoxybenzaldehyde isonicotinoylhydrazone chloroform monosolvate, and the mono- and dihydrates of 3,4,5-trimethoxybenzaldehyde isonicotinoylhydrazone: hydrogen-bonded supramolecular structures in one, two and three dimensions. Acta Crystallographica Section C-Crystal Structure Communications. 2007 Jan;63. doi: 10.1107/S0108270106052486