2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings

N  Boechat; S B  Ferreira; C  Glidewell; J N  Low; J M S  Skakle; S M S V  Wardell

doi:10.1107/S0108270105040126

2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings

N Boechat, S B Ferreira, C Glidewell, J N Low, J M S Skakle, S M S V Wardell

School of Chemistry

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Abstract

Molecules of 2-amino-5-trifluoromethyl-1,3,4-thiadiazole, C3H2F3N3S, are linked by two independent N-H (...) N hydrogen bonds into sheets of alternating R-2(2)(8) and R-6(6)(20) rings, while the molecules of the unsubstituted 2-amino-1,3,4-thiadiazole, C2H3N3S, are linked, again by two independent N-H (...) N hydrogen bonds, but into chains of edge-fused R-2(2)(8) and R-4(4)(10) rings.

Original language	English
Number of pages	3
Journal	Acta Crystallographica Section C-Crystal Structure Communications
Volume	62
DOIs	https://doi.org/10.1107/S0108270105040126
Publication status	Published - Jan 2006

Keywords

X-RAY
CRYSTAL
DIFFRACTION

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Boechat, N., Ferreira, S. B., Glidewell, C., Low, J. N., Skakle, J. M. S., & Wardell, S. M. S. V. (2006). 2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings. Acta Crystallographica Section C-Crystal Structure Communications, 62. https://doi.org/10.1107/S0108270105040126

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title = "2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings",

abstract = "Molecules of 2-amino-5-trifluoromethyl-1,3,4-thiadiazole, C3H2F3N3S, are linked by two independent N-H (...) N hydrogen bonds into sheets of alternating R-2(2)(8) and R-6(6)(20) rings, while the molecules of the unsubstituted 2-amino-1,3,4-thiadiazole, C2H3N3S, are linked, again by two independent N-H (...) N hydrogen bonds, but into chains of edge-fused R-2(2)(8) and R-4(4)(10) rings.",

keywords = "X-RAY, CRYSTAL, DIFFRACTION",

author = "N Boechat and Ferreira, \{S B\} and C Glidewell and Low, \{J N\} and Skakle, \{J M S\} and Wardell, \{S M S V\}",

year = "2006",

month = jan,

doi = "10.1107/S0108270105040126",

language = "English",

volume = "62",

journal = "Acta Crystallographica Section C-Crystal Structure Communications",

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publisher = "International Union of Crystallography",

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Boechat, N, Ferreira, SB, Glidewell, C, Low, JN, Skakle, JMS & Wardell, SMSV 2006, '2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings', Acta Crystallographica Section C-Crystal Structure Communications, vol. 62. https://doi.org/10.1107/S0108270105040126

2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings. / Boechat, N ; Ferreira, S B ; Glidewell, C et al.
In: Acta Crystallographica Section C-Crystal Structure Communications, Vol. 62, 01.2006.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - 2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings

AU - Boechat, N

AU - Ferreira, S B

AU - Glidewell, C

AU - Low, J N

AU - Skakle, J M S

AU - Wardell, S M S V

PY - 2006/1

Y1 - 2006/1

N2 - Molecules of 2-amino-5-trifluoromethyl-1,3,4-thiadiazole, C3H2F3N3S, are linked by two independent N-H (...) N hydrogen bonds into sheets of alternating R-2(2)(8) and R-6(6)(20) rings, while the molecules of the unsubstituted 2-amino-1,3,4-thiadiazole, C2H3N3S, are linked, again by two independent N-H (...) N hydrogen bonds, but into chains of edge-fused R-2(2)(8) and R-4(4)(10) rings.

AB - Molecules of 2-amino-5-trifluoromethyl-1,3,4-thiadiazole, C3H2F3N3S, are linked by two independent N-H (...) N hydrogen bonds into sheets of alternating R-2(2)(8) and R-6(6)(20) rings, while the molecules of the unsubstituted 2-amino-1,3,4-thiadiazole, C2H3N3S, are linked, again by two independent N-H (...) N hydrogen bonds, but into chains of edge-fused R-2(2)(8) and R-4(4)(10) rings.

KW - X-RAY

KW - CRYSTAL

KW - DIFFRACTION

UR - https://www.scopus.com/pages/publications/33645326213

U2 - 10.1107/S0108270105040126

DO - 10.1107/S0108270105040126

M3 - Article

SN - 1600-5759

SN - 0108-2701

VL - 62

JO - Acta Crystallographica Section C-Crystal Structure Communications

JF - Acta Crystallographica Section C-Crystal Structure Communications

ER -

Boechat N, Ferreira SB, Glidewell C, Low JN, Skakle JMS, Wardell SMSV. 2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings. Acta Crystallographica Section C-Crystal Structure Communications. 2006 Jan;62. doi: 10.1107/S0108270105040126

2-Amino-5-trifluoromethyl-1,3,4-thiadiazole and a redetermination of 2-amino-1,3,4-thiadiazole, both at 120 K: chains of edge-fused R-2(2)(8) and R-4(4)(10) rings, and sheets of R-2(2)(8) and R-6(6)(20) rings

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