Projects per year
Description
Raw 3D ED data for crystal structures included in the title publication (https://doi.org/10.1039/D5SC05651A).
Collection site University of Southampton, NCS Sample labels CCDC2415257, CCDC2415258, CCDC2415259 Instrumental
Instrument
Rigaku XtaLAB Synergy-ED, electron diffractometer Radiation source LaB6
Accelerating voltage [kV] 200
Wavelength [Å] 0.0251
Probe type Parallel beam - Beam diameter
Beam convergence Parallel beam
Detector Rigaku HyPix-ED, hybrid pixel array detector
Number of pixels in the image 775 x 385 Pixel size [µm] 100
Hardware binning
Experimental Data type Electron diffraction data - 3DED
Data collection method continuous rotation - cRED
Collection temperature [K] 175
Software
Software used for the data collection CrysAlisPro
Software used for processing CrysAlisPro
Files and data formats
Image folders ./frames/xxx.rodhypix./frames/TIFF/xxx.tiff
Image format .rodhypix (Rigaku proprietary image format).tiff (32bit, converted with CrysAlisPro 1.171.44.86a)
Additional files CrysAlisPro input files:./expinfo/./CrysalisExpSettings.ini./exp_XXX.par./exp_XXX.run./new.ccd
Collection site University of Southampton, NCS Sample labels CCDC2415257, CCDC2415258, CCDC2415259 Instrumental
Instrument
Rigaku XtaLAB Synergy-ED, electron diffractometer Radiation source LaB6
Accelerating voltage [kV] 200
Wavelength [Å] 0.0251
Probe type Parallel beam - Beam diameter
Beam convergence Parallel beam
Detector Rigaku HyPix-ED, hybrid pixel array detector
Number of pixels in the image 775 x 385 Pixel size [µm] 100
Hardware binning
Experimental Data type Electron diffraction data - 3DED
Data collection method continuous rotation - cRED
Collection temperature [K] 175
Software
Software used for the data collection CrysAlisPro
Software used for processing CrysAlisPro
Files and data formats
Image folders ./frames/xxx.rodhypix./frames/TIFF/xxx.tiff
Image format .rodhypix (Rigaku proprietary image format).tiff (32bit, converted with CrysAlisPro 1.171.44.86a)
Additional files CrysAlisPro input files:./expinfo/./CrysalisExpSettings.ini./exp_XXX.par./exp_XXX.run./new.ccd
| Date made available | 8 Jan 2025 |
|---|---|
| Publisher | Zenodo |
Projects
- 4 Finished
-
-
Light Element Analysis Facility (LEAF): Light Element Analysis Facility (LEAF)
Irvine, J. (PI), Baker, R. (CoI) & Miller, D. (CoI)
5/04/20 → 4/04/23
Project: Standard
-
H2020 ERC Advanced Grant 2017 ADOR: H2020 ERC Advanced Grant 2017 ADOR
Morris, R. (PI)
1/10/18 → 30/09/23
Project: Fellowship
Research output
- 1 Article
-
A flexible copper MOF as a carboxylate-specific crystalline sponge for structure solution using X-ray and electron diffraction
Main, R. M., Rainer, D. N., Bauzá, M., Ettlinger, R., Kelly, N. L., Coles, S. J., Ashbrook, S. E. & Morris, R. E., 14 Jan 2026, In: Chemical Science. 17, 2, p. 1116-1126Research output: Contribution to journal › Article › peer-review
Open AccessFile
Datasets
-
A flexible copper MOF as a carboxylate-specific crystalline sponge for structure solution using X-ray and electron diffraction (dataset)
Main, R. M. (Creator), Rainer, D. N. (Creator), Bauzá, M. (Creator), Ettlinger, R. (Creator), Kelly, N. (Creator), Coles, S. J. (Creator), Ashbrook, S. E. (Creator) & Morris, R. (Creator), University of St Andrews, 27 Dec 2025
DOI: 10.17630/3a837046-1fe7-43a2-9179-e8f1e87d819a
Dataset
File